U.S. patents available from 1976 to present.
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Zero order release and temperature-controlled microcapsules and process for the preparation thereof

Patent 7179407 Issued on February 20, 2007. Estimated Expiration Date: Icon_subject February 24, 2023. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Process for encapsulating particles with a silicone
Patent #: 5130171
Issued on: 07/14/1992
Inventor: Prud'Homme, et al.

Methods of encapsulating liquids in fatty matrices, and products thereof
Patent #: 5204029
Issued on: 04/20/1993
Inventor: Morgan, et al.

Method for inducing transformations in waxes
Patent #: 5209879
Issued on: 05/11/1993
Inventor: Redding, Jr.

Process for making microcapsules and apparatus therefor
Patent #: 5246636
Issued on: 09/21/1993
Inventor: Lew, et al.

Apparatus and method for making microcapsules
Patent #: 5271881
Issued on: 12/21/1993
Inventor: Redding, Jr.

Instant water dissolvable encapsulate and process Patent #: 6541030
Issued on: 04/01/2003
Inventor: Vaghefi

Inventors

Assignee

Application

No. 10373298 filed on 02/24/2003

US Classes:

264/4.1, Liquid encapsulation utilizing an emulsion or dispersion to form a solid-walled microcapsule (includes liposome)264/4.32, Microcapsule wall containing two or more layers264/4.33, Microcapsule wall derived from synthetic polymer264/4.4, Solid-walled microcapsule formed by cooling molten materials264/7, Coated particles264/9, By vibration or agitation264/12, By impinging or atomizing with gaseous jet or blast264/14, Into moving fluid428/402.24, Microcapsule with solid core (includes liposome)428/403, Coated264/432Microwave (e.g., 2.45 gigahertz, etc.)

Examiners

Primary: Staicovici, Stefan

Attorney, Agent or Firm

Foreign Patent References

  • 61242635 JP 10/01/1986
  • 2000086502 JP 03/01/2003
  • 62201635 JP 09/01/2005

International Classes

B01J 13/02
B32B 15/02

Abstract

A microcapsule composition comprising a core material in a matrix of polymorphic shell material, releases said core material in an aqueous environment in accordance with zero order linear release profile. A preferred composition comprises a core material having a degree of water solubility entrapped in a beta crystalline matrix of water insoluble shell material which matrix may, optionally, be surrounded by a contiguous core material-free layer of water insoluble shell material. Also disclosed is a process for the preparation of microcapsules comprising subjecting a flowable mixture of core material and a first amount of water insoluble shell material to a pressure force to form a pressure-treated mixture, and passing said pressure-treated mixture through a spray nozzle into a chilling zone to form a solidified composition. A special embodiment of the method providing for the long term moisture stability of the resulting microcapsules subjects the microcapsules prepared in the first step to a second coating with a second amount of water insoluble shell material.

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