U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Potassium monopersulfate triple salt with increased active oxygen content and substantially no K2S2O8

Patent 7090820 Issued on August 15, 2006. Estimated Expiration Date: Icon_subject June 28, 2024. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

2802722

2926998

3036885

Apparatus for generating an oxidizing reagent for the treatment of polluted water
Patent #: 3939072
Issued on: 02/17/1976
Inventor: LaForte

Potassium monopersulfate compositions and process for preparing them
Patent #: 4579725
Issued on: 04/01/1986
Inventor: Jayawant

Process for the production of potassium peroxymonosulphate triple salt
Patent #: 4610865
Issued on: 09/09/1986
Inventor: Reh ,   et al.

Class of stable potassium monopersulfate compositions
Patent #: 5139763
Issued on: 08/18/1992
Inventor: Amini

Process for the generation of peroxyacids
Patent #: 5141731
Issued on: 08/25/1992
Inventor: Meier, et al.

Method of preparing storage-stable aqueous sodium peroxymonsulfate solutions
Patent #: 5250280
Issued on: 10/05/1993
Inventor: Bertsch-Frank, et al.

Manufacture of peroxidic compositions
Patent #: 5429812
Issued on: 07/04/1995
Inventor: McDonogh, et al.

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Inventor

Assignee

Application

No. 10878169 filed on 06/28/2004

US Classes:

423/513, Persulfate252/186.27, Inorganic peroxide252/186.43, Contains inorganic peroxide423/521, Ternary compound containing hydrogen510/349Coated, encapsulated, or impregnated particle component in a physically heterogeneous composition (e.g., coated or encapsulated particles mixed with powder, granules, etc.)

Examiners

Primary: Anthony, Joseph D.

Attorney, Agent or Firm

International Classes

C01B 15/08
C01B 15/06

Abstract

A method of preparing a potassium monopersulfate composition is presented, wherein the potassium monopersulfate composition has the formula (KHSO5)x(KHSO4)y(K2SO4)z, where x+y+z=1 and x=0.46–0.64, y=0.15–0.37, and z=0.15–0.37, said potassium monopersulfate composition having an active oxygen content greater than or equal to 4.9 wt. % and K2S2O8 at a concentration of <0.5 wt. % of the potassium monopersulfate composition. The method includes reacting an H2O2 solution containing at least 70 wt. % H2O2 with a H2SO4 solution at a substoichiometric ratio of the H2SO4 to H2O2 to generate a weak Caro's acid solution, then combining the weak Caro's acid solution with oleum to produce a rich Caro's acid solution. The rich Caro's acid solution may be combined with an alkali potassium compound to produce the potassium monopersulfate composition. During the process, the temperature is maintained at below 30 ° C.

Other References

  • International Search Report and Written Opinion of the International Searching Authority for International application No. PCT/US04/31625 dated Jan. 18, 2006.
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