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Method of forming a nano-supported catalyst on a substrate for nanotube growth

Patent 6656339 Issued on December 2, 2003. Estimated Expiration Date: Icon_subject August 29, 2021. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Method of providing uniform emission current
Patent #: 6059627
Issued on: 05/09/2000
Inventor: Dean, et al.

Controlled synthesis and metal-filling of aligned carbon nanotubes
Patent #: 6129901
Issued on: 10/10/2000
Inventor: Moskovits, et al.

Method for manufacturing carbon nanotubes as functional elements of MEMS devices
Patent #: 6146227
Issued on: 11/14/2000
Inventor: Mancevski

Process of making bipolar electrodeposited catalysts and catalysts so made Patent #: 6346182
Issued on: 02/12/2002
Inventor: Bradley

Inventors

Assignee

Application

No. 09/942496 filed on 08/29/2001

US Classes:

205/109, Coating contains embedded solid material (e.g., particles, etc.)205/157, Coating predominantly semiconductor substrate (e.g., silicon, compound semiconductor, etc.)205/159, Coating predominantly nonmetal substrate205/162, Ceramic or glass substrate205/191, Forming nonelectrolytic coating after depositing predominantly single metal or alloy electrolytic coating205/192, Nonelectrolytic coating by vacuum or vapor deposition of a predominantly single metal or alloy coating205/193, Nonelectrolytic coating by immersion in bath of molten metal to form predominantly single metal or alloy coating (e.g., hot dipping, etc.)205/333, Oxide-containing coating (e.g., lead dioxide, etc.)423/414, CARBON OR COMPOUND THEREOF427/249.1, Carbon or carbide coating427/249.11, Hot filament utilized427/64, Fluorescent or phosphorescent base coating (e.g., cathode-ray tube, luminescent screen, etc.)427/69, Vapor deposition977/835, Chemical or nuclear reactivity/stability of composition or compound forming nanomaterial977/843, Gas phase catalytic growth (i.e., chemical vapor deposition)977/847Surface modifications (e.g., functionalization, coating, etc.)

Examiners

Primary: King, Roy V.
Assistant: Nicolas, Wesley A.

Attorney, Agent or Firm

International Classes

B01J 35/00 (20060101)
B01J 37/00 (20060101)
B01J 37/34 (20060101)
C25D 7/00 (20060101)
B01J 23/745 (20060101)
B01J 21/10 (20060101)
B01J 23/38 (20060101)
B01J 21/00 (20060101)
B01J 21/04 (20060101)
B01J 23/58 (20060101)
B01J 23/54 (20060101)
B01J 23/78 (20060101)
B01J 23/76 (20060101)

Abstract

Methods of forming a nano-supported catalyst on a substrate and at least one carbon nanotube on the substrate are comprised of configuring a substrate with an electrode (102), immersing the substrate with the electrode into a solvent containing a first metal salt and a second metal salt (104) and applying a bias voltage to the electrode such that a nano-supported catalyst is at least partly formed with the first metal salt and the second metal salt on the substrate at the electrode (106). In addition, the method of forming at least one carbon nanotube is comprised of conducting a chemical reaction process such as catalytic decomposition, pyrolysis, chemical vapor deposition, or hot filament chemical vapor deposition o grow at least one nanotube on the surface of the nano-supported catalyst (108).

Other References

  • Chen et al., "Formatio of bamboo-shaped carbon filaments and dependence of their morphology on catalyst composition and reaction conditions", Dept. of Catalysis Science and Technology, Tianjun University, China. 2001, no month avail
  • Davydov et al., "Field emitters based on porous aluminum oxide templates," Journal of Appl. Physics, vol.. 86, No. 7, Oct. 1, 1999, pp. 3983-3987
  • Database WPI, Section Ch, Week 200124, Derwent Publications, Ltd. London, AN 2002-232933, XP-002239217, Oct. 5, 2000, abstract
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