U.S. patents available from 1976 to present.
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NMR spectroscopy data recovery method and apparatus

Patent 6639405 Issued on October 28, 2003. Estimated Expiration Date: Icon_subject February 4, 2022. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

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Inventors

Assignee

Application

No. 10/067180 filed on 02/04/2002

US Classes:

324/307Using a nuclear resonance spectrometer system

Examiners

Primary: Gutierrez, Diego
Assistant: Vargas, Dixomara

Attorney, Agent or Firm

International Classes

G01R 33/46 (20060101)
G01R 33/44 (20060101)

Abstract

NMR spectroscopy data recovery methods and apparatus for improving the quality of an NMR spectrum are disclosed. The NMR spectrum is improved by acquiring more than the half spin-echo data signal and using an iterative numerical method to reconstruct the missing data points of the corresponding full symmetrical spin-echo data signal. The method includes filtering the initial data signal to extract a low-resolution phase term. The low-resolution phase term is used to form a phase-constrained initial data signal, which is Fourier-transformed to obtain a reconstructed data signal. The reconstructed data signal is modified to include the original spin-echo signal data. The formation of the reconstructed spin-echo data signal and subsequent modification is iterated until convergence is obtained. The reconstructed data signal is then Fourier-transformed to form a reconstructed NMR spectrum.

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