U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Conversion of contaminated polyethylene terephthalate to decontaminated polybutylene terephthalate

Patent 6518322 Issued on February 11, 2003. Estimated Expiration Date: Icon_subject September 1, 2020. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

3859257

Polybutylene terephthalates having a low carboxyl content and continuous process for the production thereof
Patent #: 4212963
Issued on: 07/15/1980
Inventor: Lehr ,   et al.

Process for the continuous production of polybutylene terephthalate of high molecular weight
Patent #: 4499261
Issued on: 02/12/1985
Inventor: Heinze ,   et al.

Method for producing polybutylene terephthalate
Patent #: 4656241
Issued on: 04/07/1987
Inventor: Iida ,   et al.

Process for the production of PBT carpet yarn
Patent #: 4877572
Issued on: 10/31/1989
Inventor: Clarke, et al.

Process for increasing the direct esterification reaction rate of a diacid with a glycol
Patent #: 5015759
Issued on: 05/14/1991
Inventor: Lowe

Process for preparing polybutylene terephthalate from pet scrap
Patent #: 5266601
Issued on: 11/30/1993
Inventor: Kyber, et al.

Process for the conversion of poly(ethylene terephthalate) waste to poly(alkylene terephthalate) Patent #: 5451611
Issued on: 09/19/1995
Inventor: Chilukuri, et al.

Inventor

Assignee

Application

No. 623388 filed on 09/01/2000

US Classes:

521/48.5, Treating with alcohol521/48Treating polyester

Examiners

Primary: Cain, Edward J.
Assistant: Lee, Katarzyna W.

Attorney, Agent or Firm

Foreign Patent References

  • 27 34 924 DE 02/11/1979
  • 42 20 473 DE 05/11/1994

International Class

C08J 011/04

Foreign Application Priority Data

1998-03-27 AU

Abstract

Decontaminated crushed polyethylene terephthalate is converted to decontaminated PBT withtout requiring a catalyst by mixing with 1,4-butanediol under reduced pressure, transeterifying at 120-190° C., distilling off ethanediol and tetrahydrofuran under sub-atomspheric pressure. The method lowers costs, and decreases wasteful by-products and removes contaminants present in post-consumer PET, (e.g. paper, pigments, plastics, dyes, mineral sands, and clays) and chemical and water insoluble contaminants.

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