U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Process and apparatus for liquid-liquid extraction

Patent 6413429 Issued on July 2, 2002. Estimated Expiration Date: Icon_subject January 4, 2021. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Liquid-liquid mixer
Patent #: 3973759
Issued on: 08/10/1976
Inventor: Mizrahi ,   et al.

Method for coalescence
Patent #: 4888117
Issued on: 12/19/1989
Inventor: Brown, et al.

Process for separating contaminants from organic phases during hydrometallurgical extraction of metals Patent #: 5772730
Issued on: 06/30/1998
Inventor: Bannach Sichtermann, et al.

Inventors

Assignee

Application

No. 754159 filed on 01/04/2001

US Classes:

210/634, Liquid/liquid solvent or colloidal extraction or diffusing or passing through septum selective as to material of a component of liquid; such diffusing or passing being effected by other than only an ion exchange or sorption process210/511, LIQUID AS SEPARATING MEDIUM210/513, GRAVITATIONAL SEPARATOR210/799, Filtering immiscible liquids210/800, Utilizing gravitational force210/804And additional diverse separation

Examiners

Primary: Drodge, Joseph W.

Attorney, Agent or Firm

Foreign Patent References

  • 198 15 287 DE. 10/11/1999
  • 0 685 249 EP. 12/11/1995
  • 1 443 704 GB. 07/11/1976

International Class

B02D 011/00

Foreign Application Priority Data

2000-01-07 NL

Abstract

Claimed are a process and an apparatus for extracting a component dissolved in a liquid by means of liquid-liquid extraction using an extraction liquid which is immiscible or only partially miscible with the liquid, in which process the extraction liquid is dispersed in the liquid in a dispersion apparatus and then coalesced in a coalescer, after which the ex traction liquid, the specific weight of which differs by at least 5% from the specific weight of the liquid to be extracted in which the component to be extracted is to be found, is separated from the liquid by gravity in a phase separator in which process in order to obtain an efficiency per extraction stage of at least 0.9 at an average residence time of at most 15 seconds in the dispersion apparatus and of at most 300 seconds in the phase separator, at a linear velocity in the coalescer related to its cross-section of at least 30 m/hour:a. the dispersion apparatus used is a centrifugal pump which will give droplets having an average diameter of 5 to 500 μm,b. the coalescer used is a packed bed of 5-100 cm high composed of dimensionally stable particles wettable by the extraction liquid having an average particle size of 0.05 to 2 mmL andc. the coagulated phase in the phase separator is separated at a linear velocity related to the cross-section of the phase separator of 0.1 to 0.7 times the linear velocity in the coalescer.

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