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Process for producing an isocyanurate derivative

Patent 6177541 Issued on January 23, 2001. Estimated Expiration Date: Icon_subject July 29, 2019. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Water-soluble soldering flux and paste solder using the flux
Patent #: 4988395
Issued on: 01/29/1991
Inventor: Taguchi, et al.

Resinous substance
Patent #: 5116945
Issued on: 05/26/1992
Inventor: Osawa, et al.

Method for producing purified epoxy compound Patent #: 5892065
Issued on: 04/06/1999
Inventor: Tsukamoto, et al.

Inventors

Assignee

Application

No. 362910 filed on 07/29/1999

US Classes:

528/487, Contacting with sulfur or phosphorus-containing material528/72, Reactant contains at least one phosphorus atom528/80, With reactant compound containing at least two -C-C(=X)-X-C groups and which compound is devoid of C-NH, C=NH or C-N(H)-H groups528/287, Phosphorus-containing reactant528/422, NITROGEN-CONTAINING REACTANT528/423, Reactant contains nitrogen as a ring member of a heterocyclic ring528/503Temperature maintaining, heating or cooling

Examiners

Primary: Truong, Duc

Attorney, Agent or Firm

International Classes

C08F 006/06
C08G 018/82

Foreign Application Priority Data

1998-08-20 JP

Abstract

A process for producing an isocyanurate derivative of the formula (1): ##STR1##wherein one each of X1, X2, of Y1, Y2 and of Z1, Z2, a R COO group and the other is a OH group and each R is a C1-7 organic group, having an ionic chlorine atom content of from 0.1 to 5 ppm, which comprises reacting (A) tris-(2,3-epoxypropyl) isocyanurate containing from 10 to 3,000 ppm of hydrolyzable chlorine and (B) a carboxyl group-containing compound, in the presence of (C) an arylphosphine and/or a phosphonium salt comprising a non-halogen anion, until the concentration of the epoxy group in the reaction solution decreases to a 0.3 to 0.6 eq/kg, and then maintaining the reaction solution at 80 to 130° C. for H hours, where 0.2×2,5nࣘHࣘ2×2.5n, where n=0.1(110-T), where T is the temperature (° C.), to bring the epoxy group concentration in the reaction solution to a level of less than 0.1 eq/kg.

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