Patent ReferencesWater-soluble soldering flux and paste solder using the flux Resinous substance Method for producing purified epoxy compound Patent #: 5892065 InventorsAssigneeApplicationNo. 362910 filed on 07/29/1999US Classes:528/487, Contacting with sulfur or phosphorus-containing material528/72, Reactant contains at least one phosphorus atom528/80, With reactant compound containing at least two -C-C(=X)-X-C groups and which compound is devoid of C-NH, C=NH or C-N(H)-H groups528/287, Phosphorus-containing reactant528/422, NITROGEN-CONTAINING REACTANT528/423, Reactant contains nitrogen as a ring member of a heterocyclic ring528/503Temperature maintaining, heating or coolingExaminersPrimary: Truong, DucAttorney, Agent or FirmInternational ClassesC08F 006/06C08G 018/82 Foreign Application Priority Data1998-08-20 JPAbstractA process for producing an isocyanurate derivative of the formula (1): ##STR1##wherein one each of X1, X2, of Y1, Y2 and of Z1, Z2, a R COO group and the other is a OH group and each R is a C1-7 organic group, having an ionic chlorine atom content of from 0.1 to 5 ppm, which comprises reacting (A) tris-(2,3-epoxypropyl) isocyanurate containing from 10 to 3,000 ppm of hydrolyzable chlorine and (B) a carboxyl group-containing compound, in the presence of (C) an arylphosphine and/or a phosphonium salt comprising a non-halogen anion, until the concentration of the epoxy group in the reaction solution decreases to a 0.3 to 0.6 eq/kg, and then maintaining the reaction solution at 80 to 130° C. for H hours, where 0.2×2,5nࣘHࣘ2×2.5n, where n=0.1(110-T), where T is the temperature (° C.), to bring the epoxy group concentration in the reaction solution to a level of less than 0.1 eq/kg.Field of SearchNITROGEN-CONTAINING REACTANTReactant contains nitrogen as a ring member of a heterocyclic ring Contacting with sulfur or phosphorus-containing material Temperature maintaining, heating or cooling Reactant contains at least one phosphorus atom With reactant compound containing at least two -C-C(=X)-X-C groups and which compound is devoid of C-NH, C=NH or C-N(H)-H groups Phosphorus-containing reactant | |