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US Patent 6132561 - Process for the solvent extraction for the radiolysis and dehalogenation of halogenated organic compounds in soils, sludges, sediments and slurries

US Patent Issued on October 17, 2000
Estimated Patent Expiration Date: Icon_subject October 9, 2018Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.
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Abstract

A process of extracting halogenated organic compounds, and particularly PCBs, from soil, sediment, slurry, sludge and dehalogenating the compounds contacting a contaminated soil sample with an extraction medium of a mixture of an alkane and a water miscible alcohol. The organic compounds dissolve in the extraction medium which is separated from the soil by passing water upwardly through the soil. The extraction medium floats to the surface of the water and is separated. Thereafter, the extraction medium containing the halogenated organic contaminants is subjected to ionizing radiation to radiolytically dehalogenate the compounds.

Inventors

Application

No. 168894 filed on 10/09/1998

US Classes:

204/157.15, Processes of treating materials by wave energy250/253, GEOLOGICAL TESTING OR IRRADIATION588/17, Geological or extraterrestrial588/316, Dehalogenation using reactive chemical agents able to degrade (EPO/JPO)588/318, Detoxification by using acid or alkaline reagents (EPO/JPO)588/320, By oxidation; by combustion (EPO/JPO)588/406Containing halogen (EPO/JPO)

Field of Search

588/17, Geological or extraterrestrial204/157.15, Processes of treating materials by wave energy204/164, Electrostatic field or electrical discharge436/28, In situ testing250/253, GEOLOGICAL TESTING OR IRRADIATION422/186.04Electrostatic field or electrical discharge

Examiners

Primary: Gorgos, Kathryn
Assistant: Wong, Don

Attorney, Agent or Firm

US Patent References

4144152, Dehalogenation of halogenated compounds
Issued on: 03/13/1979
Inventor: Kitchens
4842448, Method of removing contaminants from contaminated soil in situ
Issued on: 06/27/1989
Inventor: Koerner ,   et al.
5311566, In-situ x-ray treatment of organically contaminated material
Issued on: 05/10/1994
Inventor: Curry, et al.
5512253, Irradiator apparatus
Issued on: 04/30/1996
Inventor: Woodbridge, et al.
5561065, Method for testing earth samples for contamination by organic contaminants
Issued on: 10/01/1996
Inventor: Schabron
5799257Process for gamma ray induced degradation of polychlorinated biphenyls
Issued on: 08/25/1998
Inventor: Meikrantz, et al.

International Classes

C07C 001/00
A62D 003/00
G01V 005/00

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