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Ultrafine Al particle and production method thereof

Patent 6033783 Issued on March 7, 2000. Estimated Expiration Date: Icon_subject May 23, 2017. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Fine-particle metal powders Patent #: 5407458
Issued on: 04/18/1995
Inventor: Konig, et al.

Inventors

Assignee

Application

No. 861821 filed on 05/23/1997

US Classes:

428/408, SELF-SUSTAINING CARBON MASS OR LAYER WITH IMPREGNANT OR OTHER LAYER75/255, Loose particulate mixture (i.e., composition) containing metal particles148/437, Aluminum base420/528, ALUMINUM BASE502/355Of Group III (i.e., Sc, Y, Al, Ga, In or Tl)

Examiners

Primary: Wyszomierski, George

Attorney, Agent or Firm

Foreign Patent References

  • 0735001A2 EP. 10/13/1996
  • 0735001A3 EP. 07/13/1997

International Class

B32B 005/16

Foreign Application Priority Data

1996-05-27 JP

Abstract

An ultrafine Al particle consists of an Al multiply twinned particle. The Al multiply twinned particle has a decahedron structure surrounded by {111} planes. The Al multiply twinned decahedral particle has a diameter of 10 to 30 nm. Such an ultrafine Al particle consisting of the Al multiply twinned decahedral particle is obtained as follows. A metastable Al oxide particle is placed on an amorphous carbon substrate having the reduction effect. Then the electron beam is irradiated to the metastable Al oxide particle placed on the amorphous carbon substrate in the vacuum atmosphere. From the metastable Al oxide particle, Al atoms or Al clusters are emitted and adsorbed to the substrate. By adjusting the electron beam intensity so that the ultrafine Al particle in the above procedure has a diameter from 10 to 30 nm, the Al multiply twinned particle having a decahedron is obtained.

Other References

  • P. Herley et al., "Ultra-Fine Particles of Aluminium Formed by Electron-Beam-Induced Decomposition of Aluminium Hydride," Materials Letters, vol. 7, No. 12, Mar. 1989
  • B. Xu et al., "Phase Transformation and Bonding of Ceramic Nanoparticles in a Tem," NanoStructured Materials, vol. 6, pp. 727-730, 199
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