Process for recovering tantalum and/or niobium compounds from composites containing a variety of metal compounds
Patent 5787332 Issued on July 28, 1998. Estimated Expiration Date: September 26, 2016. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.
423/9, Organo-nitrogen solvent423/16, Forming peroxide (e.g., U04, etc.)423/21.1, Rare earth metal (At. No. 21, 39, or 57-71)423/21.5, Ion exchanging or liquid-liquid extracting423/68, Leaching, washing, or dissolving423/70Ion exchanging or liquid-liquid extracting
A process for treating composite materials comprising metals and having significant radioactivity for separation into concentrated individual products is provided. The process of the invention recovers valuable metals and semi-metal elements including rare earth, transition metal, radioactive elements, and compounds and composites thereof as commercially viable products while isolating the radioactive components. They key components in the composite material which are desired to be recovered are tantalum, niobium, and scandium due to their high commercial values and significant quantities. The process further includes the capability to recover uranium, thorium, rare earth, and zirconium products. Generally, the process consists of an initial sulfate roast followed by a series of hydrometallurgical unit operations designed to separate and purify the desired components into commercially usable products, such as tantalum and/or niobium in the form of metal oxides, M2 O5 ; uranium in the form of yellowcake; thorium oxalate; zirconium oxide; and rare earth sulfates.
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