U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Process of making polyester prepolymer

Patent 5786443 Issued on July 28, 1998. Estimated Expiration Date: Icon_subject December 12, 2016. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

2802028

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Process for preparing polyesters
Patent #: 4097468
Issued on: 06/27/1978
Inventor: James ,   et al.

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Inventor

Assignee

Application

No. 764370 filed on 12/12/1996

US Classes:

528/272, From di- or higher ester of a polycarboxylic acid as sole reactant, or from a polycarboxylic acid or derivative with a compound containing two or more hydroxyl groups or salts thereof526/67, REMOVING AND RECYCLING REMOVED MATERIAL FROM AN ONGOING POLYMERIZATION ZONE TO A POLYMERIZATION ZONE526/68, Recycling monomer528/274, Polymerizing in the presence of a specified material other than reactant528/296, Reactant contains three or more carboxylic acid groups or is derivative thereof528/298, Fused- or bridged-ring-containing reactant other than solely as cyclic acid anhydride group528/300, Polyhydroxy-containing compound or salt thereof having an ether-oxygen atom as reactant528/301, Acyclic ether-oxygen compound528/302, Two or more carboxylic acid or derivatives or mixtures thereof528/307, Cycloaliphatic ring-containing reactant (other than aryl)528/308, Aryl-containing carboxylic acid or derivative of an aryl-containing dicarboxylic acid528/308.6, Contains terephthalic acid or substituted forms thereof528/484, Preventing or removing reactor or processing equipment buildup528/491, Contacting with organic material528/501, With distilling or pressured reduction step to remove material, e.g., flashing, autorefrigeration, etc.528/503Temperature maintaining, heating or cooling

Examiners

Primary: Acquah, Samuel A.

International Class

C08G 063/02

Abstract

A continuous process for preparing polyester prepolymer comprising the steps of esterifying a diacid with a diol, reacting the esterified product with additional diol, and passing the product downward through a countercurrent column reactor while inert gas flows upward through the column reactor. The resulting prepolymer product has fewer acid end groups than the esterified material.

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