U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Process for the formation, isolation and purification of comestible xanthophyll crystals from plants

Patent 5648564 Issued on July 15, 1997. Estimated Expiration Date: Icon_subject December 21, 2015. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Purification of lutein-fatty acid esters from plant materials
Patent #: 4048203
Issued on: 09/13/1977
Inventor: Philip

Process for isolation, purification, and recrystallization of lutein from saponified marigold oleoresin and uses thereof Patent #: 5382714
Issued on: 01/17/1995
Inventor: Khachik

Inventors

Application

No. 576778 filed on 12/21/1995

US Classes:

568/834, Polycarbon alkyl group containing568/822, Six-membered alicyclic ring containing568/825, Single hydroxy containing (H of -OH may be replaced by a Group IA or IIA light metal)568/832, Hydroxy bonded directly to the ring (e.g., terpin hydrate, etc.) (H of -OH may be replaced by a Group IA or IIA light metal)568/913Purification or recovery

Examiners

Primary: Geist, Gary
Assistant: Puttlitz, Karl

Attorney, Agent or Firm

International Class

C07C 035/08

Abstract

A process for forming, isolating and purifying xanthophyll crystals, preferably lutein from marigold flower petals, zeaxanthin from wolfberries or capsanthin and capsorubin from red pepper, is disclosed. A xanthophyll diester-containing plant extract is saponified in a composition of propylene glycol and aqueous alkali to form xanthophyll crystals. Crystallization is achieved without the use of added organic solvents. The crystals are isolated and purified. The substantially pure xanthophyll crystals so obtained are suitable for human consumption and can be used as a nutritional supplement and as an additive in food.

Other References

  • Tyczkowski and Hamilton, Poultry Sci., 70(3): 651-654, (1991)
  • Strain, H., Leaf Xanthophylls, Carnegie Institution, Washington, D.C. (1936)
  • J. Food Sci. (1976), 41(1), 163-4. 197
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