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Method for testing earth samples for contamination by organic contaminants

Patent 5561065 Issued on October 1, 1996. Estimated Expiration Date: Icon_subject November 14, 2014. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

2451883

3149068

Field test for aromatics in groundwater
Patent #: 4992379
Issued on: 02/12/1991
Inventor: Hanby

Apparatus and method for measuring volatile constituents in earth samples
Patent #: 5050425
Issued on: 09/24/1991
Inventor: Robbins

Method for measuring volatile constituents in earth samples
Patent #: 5140845
Issued on: 08/25/1992
Inventor: Robbins

Method and means for testing soil samples
Patent #: 5181428
Issued on: 01/26/1993
Inventor: Chriswell

Detection and prevention of hydrocarbon leakage from underground storage tanks Patent #: 5344781
Issued on: 09/06/1994
Inventor: Kitchen, et al.

Inventor

Assignee

Application

No. 337897 filed on 11/14/1994

US Classes:

436/28, In situ testing422/61, Test package or kit436/31, Removing and testing solid samples436/139, HYDROCARBON436/175Digestion or removing interfering materials

Examiners

Primary: Alexander, Lyle A.

Attorney, Agent or Firm

International Class

G01N 033/24

Abstract

Provided is a method for testing earth samples for contamination by organic contaminants, and particularly for aromatic compounds such as those found in diesel fuel and other heavy fuel oils, kerosene, creosote, coal oil, tars and asphalts. A drying step is provided in which a drying agent is contacted with either the earth sample or a liquid extract phase to reduce to possibility of false indications of contamination that could occur when humic material is present in the earth sample. This is particularly a problem when using relatively safe, non-toxic and inexpensive polar solvents such as isopropyl alcohol since the humic material tends to be very soluble in those solvents when water is present. Also provided is an ultraviolet spectroscopic measuring technique for obtaining an indication as to whether a liquid extract phase contains aromatic organic contaminants. In one embodiment, the liquid extract phase is subjected to a narrow and discrete band of radiation including a desired wave length and the ability of the liquid extract phase to absorb that wavelength of ultraviolet radiation is measured to provide an indication of the presence of aromatic organic contaminants.

Other References

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