U.S. patents available from 1976 to present.
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Solar process for making fullerenes

Patent 5556517 Issued on September 17, 1996. Estimated Expiration Date: Icon_subject June 7, 2015. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Solar furnace
Patent #: 4000733
Issued on: 01/04/1977
Inventor: Pauly

Electric arc process for making fullerenes
Patent #: 5227038
Issued on: 07/13/1993
Inventor: Smalley, et al.

5236470

Inventor

Assignee

Application

No. 483045 filed on 06/07/1995

US Classes:

204/157.47, Carbon containing product produced423/445BFullerene (e.g., C60, C70, etc.)

Examiners

Primary: Lewis, Michael
Assistant: DiMauro, Peter

Attorney, Agent or Firm

Foreign Patent References

  • 9204279 WO. 03/13/1992

International Class

C01B 031/02

Abstract

This invention provides an improved process and apparatus for making fullerenes by vaporizing carbon and conducting the resulting carbon vapor to a dark zone for fullerene growth and annealing. In one embodiment concentrated solar energy is used to vaporize carbon. In a further embodiment, concentrated solar energy may be used to improve fullerene yields by vaporizing carbon and further to prevent carbon cluster formation until the carbon vapor passes into a dark zone for fullerene growth and annealing. The invention provides an improvement to increase the yield of any known process wherein carbon is vaporized under high light conditions, the improvement comprising providing a dark zone for fullerene growth and annealing.

Other References

  • Hammond et al., Ed., Fullerenes: Synthesis, Properties and Chemistry, Ch. 10-"Doping the Fullerenes," pp. 141-159 (1992)
  • Chai et al., Journ. Phys. Chem., 95(20), "Fullerenes with Metals Inside", pp. 7564-7568, Oct. 3, 1991
  • Haufler et al "Carbon Arc Generation of C60 ", Mat. Res. Soc. Symp. Proc., vol. 206 1991, pp. 627-637
  • Smalley, "Self-Assembly of Fullerenes," Acc. Chem. Res., 25(3), Mar. 1992, pp. 98-105
  • Baum, "Flood of Fullerene Discoveries continues Unabated", C & EN Jun. 1, 1992 pp. 25-33
  • IBM Technical Disclosure, vol. 34, No. 4B, Sep. 1991, p. 22
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