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Constant-depth scratch test for the quantification of interfacial shear strength at film-substrate interfaces

Patent 5546797 Issued on August 20, 1996. Estimated Expiration Date: Icon_subject April 11, 2015. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

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Patent #: 4878114
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Measurement of interfacial strength of a composite material
Patent #: 5255562
Issued on: 10/26/1993
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Scratch measurement apparatus and method Patent #: 5283642
Issued on: 02/01/1994
Inventor: Sarr

Inventors

Application

No. 422725 filed on 04/11/1995

US Classes:

73/150A, Bond strength73/81, By penetrator or indentor73/866TESTING OF MATERIAL

Examiners

Primary: Chilcot, Richard
Assistant: Noori, Max

Attorney, Agent or Firm

International Class

G01N 003/34

Abstract

A Constant-Depth Scratch Test (CDST) technique to quantitatively determine he shear strength of interfaces between thin metallic or non-metallic films and metal or ceramic substrates is revealed. The test overcomes two problems associated with other types of scratch tests, namely the instrumental complexity required for real-time detection of interfacial failure, and the inability to quantify interfacial strength. These problems are circumvented by maintaining a constant depth during scratching through the coating and the substrate, monitoring the horizontal and vertical forces to sustain the constant depth scratch, and finally by using a model to analyze the test results to quantify the interfacial shear strength. Unlike other scratch tests, this test is capable of measuring interfacial shear strength as a function of position on the film-substrate sample.

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