U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Flow regulation in gas chromatograph

Patent 5545252 Issued on August 13, 1996. Estimated Expiration Date: Icon_subject March 1, 2015. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

3496702

Flow controller-flow sensor assembly for gas chromatographs and the like
Patent #: 4096746
Issued on: 06/27/1978
Inventor: Wilson ,   et al.

Automatic chromatography apparatus
Patent #: 4802981
Issued on: 02/07/1989
Inventor: Kenney ,   et al.

Gas chromatograph having integrated pressure programmer
Patent #: 4994096
Issued on: 02/19/1991
Inventor: Klein, et al.

Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
Patent #: 5094741
Issued on: 03/10/1992
Inventor: Frank, et al.

Apparatus and methods for controlling fluids provided to a chromatographic detector
Patent #: 5108466
Issued on: 04/28/1992
Inventor: Klein, et al.

Pressure programmable gas chromatograph regulator
Patent #: 5163979
Issued on: 11/17/1992
Inventor: Patrick, et al.

Gas chromatograph and method of using same
Patent #: 5391221
Issued on: 02/21/1995
Inventor: Fukushima, et al.

Reconfigurable pneumatic control for split/splitless injection Patent #: 5431712
Issued on: 07/11/1995
Inventor: Henderson, et al.

Inventors

Assignee

Application

No. 397707 filed on 03/01/1995

US Classes:

95/15, And pressure sensed73/23.25, Temperature73/23.27, Pressure73/23.36, With electrical computer or data processor control95/22, Gas flow rate modified95/23, Gas flow rate sensed95/82, CHROMATOGRAPHY96/102, With control means responsive to sensed condition96/103, With programmed, cyclic, or time responsive control means96/105Including injection system or inlet fluid distributor

Examiners

Primary: Spitzer, Robert

Attorney, Agent or Firm

Foreign Patent References

  • 63-131059 JP 06/13/1988
  • 0546816 SU 03/13/1977

International Class

B01D 015/08

Abstract

A gas chromatographic system includes a column and an injector for delivering into the column a test portion of flow. The injector has an exit passage for discharging a split portion of carrier flow. A flow controller for regulating the inlet flow rate includes a variable outlet restrictor for the split portion, a flow rate detector disposed to detect inlet flow rate, and a feedback flow controller to regulate the outlet restrictor to maintain the inlet flow rate substantially constant. Pressure at the inlet to the injector is regulated by detecting pressure at an outlet and providing feedback control to an inlet restrictor. An integral module for the gas components is used on each side of the injector. Calibration and correction for gas characteristics are provided in the feedback for a chromatographic system and for other flow controller regulation.

Other References

  • "The Effects of Inlet Liner Configuration & Septum Purge Flow Rate on Discrimination in Splitless Injection", John Hinshaw, J. of High Resolution Chromatography 16, p. 249 (Apr. 1993)
  • "Programmed Temperature Gas Chromatography", Walter E. Harris et al, Wiley (NY), CH 2 pp. 23-29 & 46 (1966)
  • "Automatic Carrier Gas Control With Self Calibrating Capabilities" P. Magni et al in 16th Int. Symp. on Capillary Chromatography 1, p. 158 (Sep. 27, 1994)
  • "Flow Programming In Capillary Gas Chromatography", F. Poy in Frigerio et al Recent Developments In Chromatography & Electrophresis Elsevier (1979) p. 187
  • "HP 6890 Series GC System"Hewlett Packard Co. Jan. 199
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