U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Pre-thermal treatment cleaning process of wafers

Patent 5516730 Issued on May 14, 1996. Estimated Expiration Date: Icon_subject August 26, 2014. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Process for protecting polished silicon surfaces
Patent #: 4724171
Issued on: 02/09/1988
Inventor: Lampert

Method and apparatus for cleaning integrated circuit wafers
Patent #: 4863561
Issued on: 09/05/1989
Inventor: Freeman ,   et al.

Method of reducing defects on semiconductor wafers
Patent #: 4885056
Issued on: 12/05/1989
Inventor: Hall, et al.

Process for preserving the surface of silicon wafers
Patent #: 4973563
Issued on: 11/27/1990
Inventor: Prigge, et al.

Process for the wet-chemical treatment of semiconductor surfaces
Patent #: 5051134
Issued on: 09/24/1991
Inventor: Schnegg, et al.

Process for the wet-chemical surface treatment of semiconductor wafers
Patent #: 5181985
Issued on: 01/26/1993
Inventor: Lampert, et al.

Process for producing storage-stable surfaces of polished silicon wafers
Patent #: 5219613
Issued on: 06/15/1993
Inventor: Fabry, et al.

Method of characterizing the level of cleanliness of an inorganic surface
Patent #: 5275667
Issued on: 01/04/1994
Inventor: Ganesan, et al.

Wafer cleaning method and apparatus therefore
Patent #: 5288333
Issued on: 02/22/1994
Inventor: Tanaka, et al.

Surface treating cleaning method
Patent #: 5290361
Issued on: 03/01/1994
Inventor: Hayashida, et al.

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Inventors

Application

No. 296537 filed on 08/26/1994

US Classes:

438/473, By implanting or irradiating134/1.3, Semiconductor cleaning134/2, For metallic, siliceous, or calcareous basework, including chemical bleaching, oxidation or reduction134/26, Using sequentially applied treating agents257/E21.228, Wet cleaning only (EPO)257/E21.229, Combining dry and wet cleaning steps (EPO)257/E21.288, Of silicon (EPO)438/753, Silicon438/799, By differential heating438/974SUBSTRATE SURFACE PREPARATION

Examiners

Primary: Fourson, George
Assistant: Pham, Long

Attorney, Agent or Firm

International Class

H01L 021/02

Abstract

Process for heat-treating a silicon wafer which includes the steps of contacting the surface of the silicon wafer with an aqueous solution containing hydrofluoric acid to remove metals from the wafer surface, contacting the hydrofluoric acid treated wafers with ozonated water to grow a hydrophilic oxide layer on the surface of the silicon wafer, and heating the ozonated water treated wafers to a temperature of at least about 300° C. for a duration of at least about 1 second. The concentration of each of iron, chromium, calcium, titanium, cobalt, manganese, zinc and vanadium, on the surface of the silicon wafer at the initiation of the heating being less than 1×109 atoms/cm2.

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