U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Process and apparatus for the semicontinuous extraction of nicotine from tobacco

Patent 5497792 Issued on March 12, 1996. Estimated Expiration Date: Icon_subject March 12, 2013. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

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Inventors

Application

No. 122760 filed on 11/19/1987

US Classes:

131/297, Extraction of component, other than moisture, by contact with diverse medium131/298By organic solvent

Examiners

Primary: Bahr, Jennifer

Foreign Patent References

  • 1130988 CA. 07/13/1982
  • 001136 EP. 05/13/1980
  • 0088405 EP. 09/13/1983
  • 0141097 EP. 05/13/1985
  • 397021 FR. 02/13/2012
  • 2106252 FR. 04/13/1972
  • 3716689 DE. 01/13/1988
  • 82835 LU. 02/13/1987
  • 0028536 GB 02/13/2012

International Class

A24B 015/24

Abstract

A process is provided for the improved removal of nicotine from tobacco. An essentially nicotine-free solvent in the supercritical or liquid state is fed into a first end of an extraction flow system containing tobacco and a nicotine-rich solvent is discharged from a second end of the extraction flow system. Periodically a portion of extracted tobacco is discharged from the first end of the extraction system while simultaneously a portion of an unextracted tobacco is charged to the second end of the extraction system. Nicotine is then entrapped in an entrapment material or otherwise removed from the solvent and solvent is recycled through the extraction flow system. Various materials are provided as entrapment materials. Among the entrapment materials provided are aqueous solutions containing absorbent selected from various acids and salts. Among the acids and salts provided as entrapment materials are sulfuric acid, phosphoric acid, nitric acid, tartaric acid, citric acid, malic acid, lactic acid, malonic acid, succinic acid, acetic acid, glutamic acid and monopotassium citrate.

Other References

  • P. Hubert & O. G. Vitzhthum, "Fluid Extraction of Hops, Spices, and Tobacco with Supercritical Gases", Angewandte Chemie, Int. Ed. Engl. 17, pp. 710-715 (1978)
  • D. F. Williams, "Extraction With Superficial Gases", Review Article No. 5, Chemical Engineering Science 36 pp. 1769-1788, 1781 (1981)
  • L. N. Luganskaja, E. B. Krasnokutskaj and L. B. Jasinskaja, "The Use Of Tobacco Dust Extract For Aromatizing Purposes", Tabak, SSSR 1, pp. 30-33 (1967) (translation enclosed
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