U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Method for making moisture insensitive zinc sulfide based luminescent materials

Patent 5080928 Issued on January 14, 1992. Estimated Expiration Date: Icon_subject October 5, 2010. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Method for coating phosphor particles
Patent #: 4585673
Issued on: 04/29/1986
Inventor: Sigai

Electroluminescent lamps and phosphors Patent #: 4855189
Issued on: 08/08/1989
Inventor: Simopoulos ,   et al.

Inventors

Assignee

Application

No. 593451 filed on 10/05/1990

US Classes:

427/70, Nonmetallic coating formed by vapor deposition427/66, Electroluminescent lamp427/69, Vapor deposition427/213, Fluidized bed utilized427/215, Inorganic base427/220, Organic coating427/255.395, Inorganic coating427/255.6Organic coating applied by vapor, gas, or smoke

Examiners

Primary: Beck, Shrive
Assistant: Burke, Margaret

Attorney, Agent or Firm

Foreign Patent References

  • 175567 JP. 07/13/1986
  • 63-224943 JP. 03/13/1987
  • 1110955 JP. 10/13/1987

International Classes

B05D 005/12
B05D 007/00
C23C 016/00
C23C 016/44

Abstract

A process is disclosed for coating phosphors with hydrolyzed alkylaluminum. The hydrolyzed alkylaluminum coating renders the phosphors insensitive to atmospheric moisture. the coating process involves vaporizing an aluminum-containing precursor such as trimethylaluminum or triethylaluminum in an inert gas stream and passing this through a fluidized bed containing the phosphor particles. Water vapor is also passed through the fluidized bed and the water and aluminum precursor react on the surface of the phosphor particles to form hydrolyzed trimethylaluminum or other alkylaluminum. The hydrolyzed trimethylaluminum or other alkylaluminum phosphors are particularly useful in electroluminescent lamps.

Other References

  • A. G. Fisher et al., Advances in AC-Electroluminescent Powder Layers, SPIE vol. 99 3rd European Electro-Optics Conf. (1976) pp. 202-208
  • S. Roberts, Aging Characteristics of Electroluminescent Phoshors, Jour. of Appld. Phys. vol. 28, No. 2, Feb. 1957 pp. 262-265
  • W. A. Thornton, Electroluminescence Maintence, J. of Electrochemical Soc., vol. 107, No. 11, (Nov. 1960) pp. 895-907
  • K. Wefers, G. M. Bell "Oxides and Hydroxides of Aluminum" Tech. Paper 19, Alcoa Research Lab., East St. Louis, 111 1972
  • T. A. Mole, E. A. Jeffery, "Organoaluminium Compounds" Elsevier Publishing Co, Amsterdam, 1972 Chapter
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