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Method of manufacturing spherical silica particles

Patent 5028360 Issued on July 2, 1991. Estimated Expiration Date: Icon_subject April 16, 2010. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

Process for producing silica in fine powder form
Patent #: 4678652
Issued on: 07/07/1987
Inventor: Tamenori ,   et al.

Process for manufacturing high purity silica
Patent #: 4683128
Issued on: 07/28/1987
Inventor: Orii ,   et al.

Spherical silica glass powder particles and process for their production
Patent #: 4767433
Issued on: 08/30/1988
Inventor: Iura ,   et al.

Process for producing unsintered cristobalite silica
Patent #: 4853198
Issued on: 08/01/1989
Inventor: Orii ,   et al.

Process for preparing precipitated silica
Patent #: 4857289
Issued on: 08/15/1989
Inventor: Nauroth ,   et al.

Process for producing silica of high purity
Patent #: 4857290
Issued on: 08/15/1989
Inventor: Shimizu

Porous structures Patent #: 4913966
Issued on: 04/03/1990
Inventor: Garvey, et al.

Inventors

Assignee

Application

No. 508813 filed on 04/16/1990

US Classes:

264/12, By impinging or atomizing with gaseous jet or blast264/13, By extrusion spraying or gravity fall through orifice264/621, Utilizing sol or gel423/335, Silica423/338, By gelling423/339By precipitating

Examiners

Primary: Theisen, Mary Lynn

Attorney, Agent or Firm

Foreign Patent References

  • 50-67797 JP 06/13/1975
  • 58-2233 JP. 01/13/1983
  • 58-145613 JP. 08/13/1983
  • 60-131868 JP. 07/13/1985
  • 61-251509 JP. 11/13/1986
  • 62-3011 JP. 01/13/1987
  • 62-79841 JP. 04/13/1987
  • 62-96308 JP. 05/13/1987
  • 62-96309 JP. 05/13/1987
  • 62-96311 JP. 05/13/1987
  • 62-96312 JP. 05/13/1987
  • 62-96313 JP. 05/13/1987
  • 62-283809 JP. 12/13/1987
  • 63-225538 JP. 09/13/1988

International Classes

B29B 009/10
C01B 033/12
C01B 033/18

Foreign Application Priority Data

1989-04-17 JP

Abstract

A method of manufacturing spherical silica particles comprising the steps of processing in an acid-containing solution and then washing with water the coagulant derived from an aqueous alkali metal silicate solution extruded through pores in a water-miscible organic medium or acid solution, wet-grinding the amorphous silica thus obtained in a liquid dispersion medium to obtain a fine particle silica suspension with a weight average particle size of 10 μm or less, spray-drying this fine particle silica suspension with hot air and sintering the spherical granulated silica thus obtained. According to the present invention, the high-purity spherical silica particles can be obtained with high solidity and adjusted surface smoothness without any complicated operation or waste water treatment for use as a sealant filler for highly-integrated IC electronic parts.

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