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US Patent 4950310 - Process for the preparation of crystalline sheet sodium silicates

US Patent Issued on August 21, 1990
Estimated Patent Expiration Date: Icon_subject December 8, 2008Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.
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Abstract

X-ray crystalline sodium silicates having a sheet structure and an SiO2 :Na2 O molar ratio of 1.9 to 3.5 are prepared by dissolving an X-ray crystalline sodium silicate having a sheet structure and an SiO2 /Na2 O molar ratio of 1.9:1 to 3.5:1 in water and evaporating the solution at temperatures of 20° to 445° C.For the preparation of detergents or cleaners, a mixture of surfactants and builders, which may also contain fillers, bleaching agents, bleach activators and enzymes, is made into a paste with water, mixed with an X-ray crystalline sheet sodium silicate having an SiO2 /Na2 O molar ratio of 1.9:1 to 3.5:1, mixed thoroughly and then spray-dried.

Other References

  • A. Willgallis et al., Glastechn. Ber. 37, 194-200 (1964)
  • Gmelins Handbuch der Anorganischen Chemie, 8th Ed., Part C ("Phosphorus"), System No. 16, Vergal Chemie, Weinheim, 1965, p. 259
  • K. Beneke et al., Am. Minerol., 62, 763-771 (1977

Inventors

Application

No. 281805 filed on 12/08/1988

US Classes:

23/295R, Crystallization23/303, Common salt423/332, Alkali metal containing (Li, Na, K, Rb, or Cs)423/333By precipitating or gelling from silicate solution

Field of Search

423/332, Alkali metal containing (Li, Na, K, Rb, or Cs)423/333, By precipitating or gelling from silicate solution23/295R, Crystallization23/303Common salt

Examiners

Primary: Nucker, Christine M.
Assistant: Steffe, Eric

US Patent References

4166039, Detergent composition and process
Issued on: 08/28/1979
Inventor: Wise
4478735, Process for producing granular detergent composition
Issued on: 10/23/1984
Inventor: Yazaki ,   et al.
4524010, High-sudsing, granular detergent composition with greater granulate stability and process for its preparation
Issued on: 06/18/1985
Inventor: Reuter ,   et al.
4585642, Process for the preparation of crystalline sodium silicates
Issued on: 04/29/1986
Inventor: Rieck
4632815, Crystalline layered silicate
Issued on: 12/30/1986
Inventor: Valyocsik
4664839, Use of crystalline layered sodium silicates for softening water and a process for softening water
Issued on: 05/12/1987
Inventor: Rieck
4737306Layered silicates of limited swelling power, a process for their production and their use in detergents and cleaning preparations
Issued on: 04/12/1988
Inventor: Wichelhaus ,   et al.

Foreign Patent References

  • 0164552 EP 11/21/1985
  • 3413571 DE 04/21/1984
  • 3417649 DE 11/21/1985

International Class

C01B 033/02

Foreign Application Priority Data

1987-12-11 DE

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