U.S. patents available from 1976 to present.
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Miniature devices useful for gas chromatography

Patent 4935040 Issued on June 19, 1990. Estimated Expiration Date: Icon_subject March 29, 2009. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

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Inventor

Assignee

Application

No. 330246 filed on 03/29/1989

US Classes:

73/23.22, For gas chromatography96/104, Plural separate and distinct stages96/417, WITH SIGNALS, INDICATORS, MEASURING, OR TESTING MEANS210/198.3Thin layer, e.g., plate, etc.

Examiners

Primary: Spitzer, Robert

Attorney, Agent or Firm

Foreign Patent References

  • 60-142254 JP 07/13/1985
  • 60-229342 JP 10/13/1985
  • 61-142462 JP 06/13/1986
  • 61-176853 JP 08/13/1986
  • 61-233365 JP 10/13/1986
  • 61-233366 JP 10/13/1986
  • 61-288154 JP 12/13/1986
  • 63-098561 JP 04/13/1988
  • 399780 CH 03/13/1966

International Classes

B01D 015/08
G01N 030/66

Abstract

Laminated wafers with channels formed therein define a plurality of gas chromatographic columns in a body, with substantially minimal connecting channels between an injector and a detector. One or more of the columns at a time is selected by valve to be receptive of sample gas. Detector and injector cavities have surfaces with the adsorbent phase utilized in the column being further coated on the surfaces, whereby the detector and injector constitute an integral portion of the gas chromatographic column. A channel is formed between wafers each with grooves that have semicircular cross sections so as to form the channel with a circular cross section. A digital gas injector includes a plurality of chambers with respective measured volumes. Valves select one or more of the chambers at a time to be receptive of sample gas from the common inlet. A detector comprises a body having a passage therein receptive of a first flow consisting of a sample gas mixed into a carrier gas, and alternatively receptive of a second flow consisting of a reference gas. Preferably the first and second flows are oppositely directed by valves alternatively through the passage. Boron or silicon nitride film is utilized in cavities in the body so as to provide a structural component for membranes of the valves and for hot wire detectors.

Other References

  • "A Prototype Gas Analysis System Using a Miniature Gas Chromatograph" by J. H. Jerman, S. C. Terry and S. Saadat, Stanford University, Jun. 2, 1980
  • "Silicon as a Mechanical Material" by K. E. Peterson, Proc. IEEE 70, 420-457, May 1982
  • "A Microminiature Electric-to Fluidic Valve" by M. J. Zdeblick and J. B. Angell, Transductors 87, pp. 827-829 (1987)
  • "Boron Nitride Mask Structure for X-Ray Lithography" by D. Maydan, G. A. Coguin, H. J. Levinstein, A. K. Sinha and D. N. K. Wang, J. Vac. Sci Technol 16 1959-61 (Nov./Dec.) 197
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