U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Method for making N-substituted nitrophthalimides

Patent 4902809 Issued on February 20, 1990. Estimated Expiration Date: Icon_subject February 20, 2007. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

3415876

3868389

3920697

Process for making N-methyl nitrophthalimides
Patent #: 3933852
Issued on: 01/20/1976
Inventor: Cook ,   et al.

Process for making dinitrotoluene
Patent #: 3981933
Issued on: 09/21/1976
Inventor: Cook ,   et al.

Method for making n-alkylphthalimides
Patent #: 4020089
Issued on: 04/26/1977
Inventor: Markezich

Process for the production of nitro derivatives of aromatic compounds
Patent #: 4036838
Issued on: 07/19/1977
Inventor: Vogel ,   et al.

Process for the production of aromatic mononitro compounds
Patent #: 4064147
Issued on: 12/20/1977
Inventor: Thelen ,   et al.

Process for the preparation of mononitro-aromatic compounds
Patent #: 4112005
Issued on: 09/05/1978
Inventor: Thiem ,   et al.

Destruction of DNPI in an all nitric acid nitration process Patent #: 4599429
Issued on: 07/08/1986
Inventor: Odle

Inventors

Application

No. 917926 filed on 10/10/1986

US Classes:

548/481Chalcogen or nitrogen attached indirectly to ring carbon of the bicyclo ring system by acyclic nonionic bonding

Examiners

Primary: Ceperley, Mary E.

Attorney, Agent or Firm

Foreign Patent References

  • 0108604 EP. 05/13/1984
  • 2270247 FR. 12/13/1975
  • 329367 CH. 06/13/2012
  • 635635 GB. 04/13/2012

International Class

C07D 209/48

Abstract

A process for preparing N-alkyl substituted nitrophthalimide by the nitration of N-alkyl substituted phthalimide using only nitric acid, said nitric acid having a concentration of at least about 95%, and then recovering N-alkyl nitrophthalimide from the nitric acid solution.

Other References

  • Hughes et al., "Kinetics and Mechanism of Aromatic Nitration Part II", pp. 2400-2440, 1949
  • Shofield, K., "Aromatic Nitration", Cambridge University Press, pp. 23-43, 1980
  • Astle, M. J., "Industrial Organic Nitrogen Compounds", Reinhold Publishing Corp., pp. 314-344, 1961, p. 459, 1943
  • Houben-Weyl, Methoden der Organischen Chemi, vol. X/1, part 1, 1971, George Thieme Verlag (Stuttgart, DE), pp. 622-623
  • Gordon et al, "The Chemist's Companion", John Wiley and Sons, p. 152 (1972)
  • Blatt, A. H., ed., "Organic Synthesis", Collective vol. 2, John Wiley and Sons, p. 459 (1943)
  • Methods of Organic Chemistry (Houben-Weyl), vol. X/1, Nitrogen Compounds I, Part 1, Fourth Ed., pp. 622-624
  • C. Noller, Chemistry of Organic Compounds, Second Edition, W. B. Saunders Co., Philadelphia, QD253N65
  • Gordon et al, The Chemist's Companion, John Wiley and Sons, p. 152 (1972)
  • Albright et al, Ed., Industrial and Laboratory Nitrations, ACS, pp. 48, 49 (1976)
  • Blatt, A. H., Ed., Organic Synthesis, Coll. vol. 2, John Wiley and Sons, p. 459 (1943)
  • March, Jerry, Advanced Organic Chemistry, second edition, McGraw-Hill, NY (1977), pp. 388-389, 474-47
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