U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Total organic carbon analyzer

Patent 4619902 Issued on October 28, 1986. Estimated Expiration Date: Icon_subject July 27, 2004. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

3784359

3864088

Analytical method and apparatus for determination of total nitrogen and/or carbon contents in aqueous systems
Patent #: 4066402
Issued on: 01/03/1978
Inventor: Komiyama ,   et al.

Analytical method for the determination of nitrogen, carbon, hydrogen and sulfur or chlorine and apparatus therefor Patent #: 4401763
Issued on: 08/30/1983
Inventor: Itoh

Inventor

Application

No. 06/635147 filed on 07/27/1984

US Classes:

436/145, CARBON CONTAINING422/78, Including means for pyrolysis, combustion, or oxidation422/79, Biological, chemical, or total oxygen demand (i.e., BOD, COD, TOD)422/80, And means directly analyzing evolved gas436/146In an aqueous solution (e.g., TOC, etc.)

Examiners

Primary: Chin, Peter

Attorney, Agent or Firm

International Classes

G01N 33/18 (20060101)
G01N 31/00 (20060101)

Abstract

An improved digestion chamber (10) is provided for use in a carbon analysis system. A catalyst (16), selected from the platinum metals group consisting of platinum, rhodium, palladium, osmium, iridium and ruthenium, provides an oxidizing surface for the sample being analyzed. The oxidant (26) is preferably persulfate, which may be stored in a generally stable solution until needed for sample oxidation. The catalyst (16) may be provided as a digestion chamber wire insert, such as a rod or as a plating on the chamber walls, enabling an increased variety of materials to be used for the vessel. In a preferred embodiment of the digestion chamber, polytetrafluoroethylene is used to reduce the background carbon which must be corrected in the analysis.

Other References

  • Baldwin and McAtee, "Determination of Organic Carbon in Water with a Silver-Catalyzed Peroxydisulfate Wet Chemical Oxidation Method", 19 Microchem. J. 179 (1974)
  • Osburn and Werkman, "Determination of Carbon in Fermented Liquors", Ind. and Eng. Chem. 421 (1932)
  • Menzel and Vaccaro, "The Measurement of Dissolved Organic and Particulate Carbon in Seawater", 9 Limnol. Oceanogra. 138 (1964)
  • Goulden and Brooksbank, "Automated Determinations of Dissolved Organic Carbon in Lake Water", Anal. Chem. 1943 (1975)
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