Patent References 2901318 2901319 3036885 3041139 InventorAssigneeApplicationNo. 06/771490 filed on 09/04/1985US Classes:423/513PersulfateExaminersPrimary: Straub, Gary P.International ClassesC01B 15/00 (20060101)C01B 15/08 (20060101) AbstractA storage stable salt melting at 80° to 150° C. having the formula (KHSO5)x (KHSO4)y (K2 SO4)z where x+y+z=1, and x=0.4-0.97, preferably 0.60-0.85; y=0.03-0.60, preferably 0.15-0.40; z=0-0.10, preferably 0-0.3; and y is ࣙz, which is treated with 1.0-9.0% of a basic magnesium compound which is MgCO3, Mg(OH)2, MgO or mixtures thereof is disclosed. The salt is prepared by neutralizing Caro's acid with a basic potassium compound to form a reaction mixture. Water is evaporated from the reaction mixture at 15° to 35° C. using a vacuum of 2-15 mm Hg absolute pressure to form up to 40 wt. % crystals. The crystals are separated, treated with a basic magnesium compound, dried, and further treated with a basic magnesium compound.Field of SearchPersulfate |
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