U.S. patents available from 1976 to present.
U.S. patent applications available from 2005 to present.

Process for producing sodium carbonate from complex brines

Patent 4291002 Issued on September 22, 1981. Estimated Expiration Date: Icon_subject September 22, 1998. Estimated Expiration Date is calculated based on simple USPTO term provisions. It does not account for terminal disclaimers, term adjustments, failure to pay maintenance fees, or other factors which might affect the term of a patent.

Patent References

1865833

2693403

2962348

3028215

3188170

3717698

3900292

Inventors

Assignee

Application

No. 05/844847 filed on 10/25/1977

US Classes:

423/189, Utilizing carbon dioxide as reactant423/190, Mixture contains metal chloride423/422, Hydrogen containing (bicarbonate)423/426, Densifying soda ash423/427By reacting a bicarbonate

Examiners

Primary: Vertiz, O. R.
Assistant: Langel, Wayne A.

Attorney, Agent or Firm

International Class

C01D 7/00 (20060101)

Abstract

A process for the production of sodium carbonate wherein sodium bicarbonate is recovered from a brine containing sodium carbonate by carbonation of the brine under controlled conditions. The sodium bicarbonate is crystallized from the carbonated brine in a multi-stage carbonating, cooling and crystallization process after which it is filtered to produce wet cake. The wet cake is subjected to predrying to provide a predried wet cake of a specified free moisture content and mixed with recycle light ash to provide a dryer feed of specified moisture content to alleviate problems of product fouling or plugging of the dryer. The light ash from the dryer then is bleached and subjected to recrystallization, screening, centrifuging and drying to provide a dried sodium carbonate possessing, after evaporation of the water of hydration and free moisture, less than 0.10 percent moisture and chemical and physical properties meeting commercial dense ash specifications.

Other References

  • Manufacture of Soda by Te-Pang Hou, Ph.D., Reinhold Publishing Corporation (1942), pp. 173-179
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