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Class 548/555 - Purification or recovery of 2-pyrrolidone which is unsubstituted or alkyl substituted only


Subclass of Class 548 - Organic compounds -- part of the class 532-570 series
Definition: Processes wherein 2-pyrrolidone, which is unsubstituted
No. of patents: 48
Last issue date: 05/22/2012


1    
NumberTitleIssue Date
8183389Process for the treatment of an aqueous mixture comprising a dipolar aprotic compound
The invention relates to a process for the treatment of an aqueous mixture comprising a dipolar aprotic compound, comprising: a) an adsorption step, in which the aqueous mixture is brought into contact with a porous adsorbent, whereby the porous adsorbent is chosen ...
05/22/2012
7947845Process for purifying removal of acrylic acid, methacrylic acid N-vinylpyrrolidone or P-xylene crystals from their suspension in mother liquor
A process for purifying removal of acrylic acid, methacrylic acid, N-vinylpyrrolidone or p-xylene crystals from their suspension in mother liquor by means of a wash column with forced transport, whose shell of the process chamber is a metal wall, the wash column add...
05/24/2011
7732624Process for operating a continuous removal of a target product X in the form of fine crystals
A process for continuously removing a target product X in the form of fine crystals from a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in an indirect heat transferer, in which ...
06/08/2010
7153978Method for purifying N-methyl-2-pyrrolidone
A method for purifying N-methyl-2-pyrrolidone is disclosed. The method comprises treating N-methyl-2-pyrrolidone with an alumina that desorbs less than 100 μmol/g of isobutylene between 225° C. and 400° C. in a standard tert-butyl alcohol dehydration test. The me...
12/26/2006
7138528Method for crystallizing N-vinyl-2-pyrrolidone
A method for purifying N-vinyl-2-pyrrolidone (NVP) is disclosed. The method comprises crystallizing NVP in the presence of added water to produce purified NVP crystals and a mother liquor, and then isolating the purified crystals. In a preferred method, 0.5 to 4 wt....
11/21/2006
7129376Method for the production of a purified melt of at least one monomer
The invention relates to a method for the production of a purified melt of a monomer melt obtained by condensation, absorption or extraction in a crystallizer, wherein the inlet to the crystallizer is subjected to a mechanical solid/liquid separation operation. ...
10/31/2006
7037412Method for preparing deodorized N-vinyl-2-pyrrolidone
The invention provides a method for producing purified N-vinyl-2-pyrrolidone free of odorous components. The method is composed of distilling with a distillation column a liquid, which is formed by adding to an odorous components-containing liquid having a N-vinyl-2...
05/02/2006
6888006Method for processing pyrollidone and n-vinyl pyrollidone residues
A process for working up residues from the preparation of pyrrolidone and/or N-vinylpyrrolidone comprises subjecting the residues to a thermolysis. ...
05/03/2005
6726811Method of purifying N-(2-hydroxyethy)-2-pyrrolidone
A method for obtaining high purity N-(2-hydroxyethyl)-2-pyrrolidone satisfactory for use as an intermediate material for N-vinyl-2-pyrrolidone from a reaction liquid formed of a reaction between y-butyrolactone and 2-aminoethanol, i.e., a liquid containing N-(2-hydr...
04/27/2004
6703511Method for obtaining pure n-vinyl pyrrolidone
The invention describes a process for the isolation of pure N-vinylpyrrolidone from N-vinylpyrrolidone-containing crude products, comprising a single-stage or multistage crystallization process, which comprises passing the mother liquor from the first cry...
03/09/2004
6521097Process for separating hydrogen chloride from a mixture comprising an N-alkyl-2-pyrrolidone and hydrogen chloride
A process for separating hydrogen chloride from a mixture including an N-(C1 -C18)-alkyl-2-pyrrolidone and hydrogen chloride by distilling the mixture including an N-(C1 -C18)-alkyl-2-pyrrolidone and hydrogen ch...
02/18/2003
6486169Botanical drug for treatment and prevention of alzhimer's disease
The present invention related to safe botanical drug for treatment and prevention of Alzheimer's disease. Specifically, this invention proves a safe botanical drug, Huperzine (HUE) and Clausenamide (CLE) and their preparation. HUE has the following pharma...
11/26/2002
6436243Process for recovering N-vinyl-2-pyrrolidone
A process for recovering N-vinyl-2-pyrrolidone is provided which allows to recover N-vinyl-2-pyrrolidone efficiently and steadily and in high purity by continuous distillation from a mixed liquid containing N-vinyl-2-pyrrolidone, N-(2-hydroxyethyl)-2-pyrr...
08/20/2002
6417356Stabilization of vinylether and vinyl lactam formulations against hydrolysis
This invention relates to a composition containing (a) a component selected from the group of a mono- or poly- vinyl substituted mono- or poly-ether, a mono- or poly- vinyl substituted lactam, or a mixture thereof contained in an acidic medium and (b) an ...
07/09/2002
6207824Purification of N-substituted lactams
A process for reducing the amine content of amine-contaminated N-substituted lactams comprises treating the contaminated N-substituted lactams with an acid macroporous cation exchanger....
03/27/2001
6051720Removal of contaminants from N-methyl-2-pyrrolidone
A process is provided for moving at least one contaminant selected from the group consisting of phenol thiophenol, and phenyl disulfide from contaminated NMP by reacting at least one monohalogenated aromatic compound and a base with the contaminate NMP....
04/18/2000
5945544Process for production of N-vinyllactam
A process for producing an N-vinyllactam by reacting a lactam with acetylene in the presence of a particular catalyst (an alkali metal alcoholate between an alicyclic alcohol and an alkali metal) in a nonaqueous system at an acetylene partial pressure of ...
08/31/1999
5777131Post manufacture process for improving the properties of lactones and substituted lactams
This invention relates to a method for improving the properties of lactones and substituted lactams by subjecting the post-manufactured lactones and substituted lactams to an ion exchange resin. Specifically, this invention relates to a method for reducin...
07/07/1998
5710284Purification of N-vinylpyrrolidone by crystallization
In a process for purifying N-vinylpyrrolidone by crystallization in a crystallizer, those surfaces of the crystallizer from which crystals grow during the crystallization are covered with an N-vinylpyrrolidone seed layer before the crystallization....
01/20/1998
5462643Method for reprocessing solvent mixtures containing constituents of low volatility and apparatus suitable therefor
Reprocessing mixtures which contain organic solvents and constituents of low volatility and may contain water: includes introducing the mixture into a concentration apparatus of a solvent recovery system, concentrating the mixture in the concentration app...
10/31/1995
5461159Binding chemical impurities contained in crude N-vinylpyrrolid-2-one
Chemical impurities contained in N-vinylpyrrolid-2-one are bound by a process in which the anhydride of an organic carboxylic acid is added to the crude N-vinylpyrrolid-2-one....
10/24/1995
5183538Extraction plus ion exchange processing of a brine stream
A method for recovering a liquid diluent having a low salt content from an organic/aqueous mixture which contains significant quantities of the diluent, an alkali metal salt, and water comprises an integrated process which joins extraction and ion exchang...
02/02/1993
5167775Method for recovery of solvent used in production of polyarylene sulfide
The present invention provides a method for the recover of a solvent used in the production of a polyarylene sulfide according to which the deterioration of the solvent is low and the recovery rate is high, wherein a mixed liquid, mainly composed of the s...
12/01/1992
5068358Process for extracting N-methyl-2-pyrrolidone
The invention relates to a process for separating N-methyl-2-pyrrolidone (NMP) from aqueous solutions which are obtained in industry, inter alia, in the production of heat-resistance polymers such as polyamides and polyimides. According to the invention, ...
11/26/1991
5039817Preparation of pure N-vinyl-2-pyrrolidone
Pure N-vinyl-2-pyrrolidone is prepared by treating the crude N-vinyl-2-pyrrolidone with an acid ion exchanger....
08/13/1991
4976825Process for recovering N-methylpyrrolidone by plural distillations
A process for recovering N-methylpyrrolidone contained in an N-methylpyrrolidone-containing liquid formed in the process for preparing a polyarylene thioether by the dehalogenosulfidation of a dihalogeno-aromatic compound and an alkali metal sulfide in th...
12/11/1990
4965370N-methyl-2-pyrrolidone purification
A process for recovering N-methyl-2-pyrrolidone from an effluent stream in a poly(arylene sulfide) process containing N-methyl-2-pyrrolidone contaminated with acidic compounds and high boiling contaminants by contacting the kettle liquid from a heavies fr...
10/23/1990
4895959Purification of N-methyl-2-pyrrolidone
A method for purifying N-methyl-2-pyrrolidone containing thiophenol and/or diphenyl disulfide is disclosed, comprising adding a polyhalogenated aromatic compound and an alkali metal hydroxide and/or an alkali metal carbonate to the N-methyl-2-pyrrolidone ...
01/23/1990
4859781Recovery of N-methyl-2-pyrrolidone
In a process for recovery N-methyl-2-pyrrolidone from a liquid aqueous medium (preferably a brine) by liquid-liquid extraction, the improvement comprises using a branched aliphatic C5-C7 alcohol as extractant. In a particular embodiment, the liquid aqueou...
08/22/1989
4837338Removal of impurities from n-methyl-pyrrolidone using highly pure water washed activated alumina
N-methyl pyrrolidone solvent (hereinafter NMP) used to extract aromatic components from lubricating oil distillates is purified by contacting the solvent with activated alumina....
06/06/1989
4831160Removal of volatile acids from NMP solvent vapors with sacrificial metal and ion exchange
Volatile acids present in n-methyl pyrrolidone vapor from solvent extraction processes can be reacted with sacrificial metals such as magnesium to concentrate the acid salts into a small volume of oil/NMP. Steam stripping removes NMP from the oil/NMP mixt...
05/16/1989
4610768Lactam purification
A process for drying lactams to extremely low water contents is provided which comprises mixing the lactam with hydrocarbon distilling from the mixture a water/hydrocarbon vapor and or condensate, contacting said vapor or condensate with a drying agent to...
09/09/1986
4552970Solvated salts of dinitrophenylcyanamides, and a process for the preparation thereof
Compounds of the formula I ##STR1## in which X denotes hydrogen, fluorine, chlorine or bromine, Y and Z denote hydrogen, lower alkyl or lower alkoxy, M denotes sodium, potassium or one equivalent of calcium and L denotes a dipolar aprotic solvent, ar...
11/12/1985
4510316Purification of N-methylpyrrolidone
Phenol is extracted with a chlorinated aromatic extractant, such as p-dichlorobenzene, from an aqueous mixture containing phenol and N-methylpyrrolidone. In an embodiment of this invention the purified N-methylpyrrolidone is recycled for use in a poly(phe...
04/09/1985
4501902N-Methyl pyrrolidone-2 purification
A process for removing compounds from aprotic solvents in which aprotic solvent containing at least one acidic compound is contacted with a solid inorganic compound chosen from alkaline earth carbonates, alkaline earth hydroxides, alkaline earth oxides, a...
02/26/1985
4472585Extraction of N-methylpyrrolidone-2
Water or acidified water can be used to extract N-methylpyrrolidone from a mixture containing phenol and N-methylpyrrolidone. In one embodiment of this invention water or acidified water can be used to extract N-methylpyrrolidone from the kettle bottoms o...
09/18/1984
4400521N-Substituted phenyl maleimides
Maleimide compounds represented by the general formula (I) ##STR1## where R and R' are a hydrogen atom, a halogen atom, or an alkyl radical of from 1 to 4 carbon atoms, and n and n' are a whole number of from 1 to 4; and a process for the preparation...
08/23/1983
4384125Process for the purification of 2-pyrrolidone
In a distillation process 2-pyrrolidones obtained from succinonitrile are purified by treating the impure liquid pyrrolidone with a strong base, fractionally distilling this product to yield, as distillate, polymerization grade purified 2-pyrrolidone, mix...
05/17/1983
4316846Recovery of aprotic amides
The present invention relates to the recovery of three aprotic amide solvents from their water solutions by extraction with a selected class of organic solvents characterized generally by having two electron withdrawing substituents, exemplified by fluori...
02/23/1982
4276215Purification of pyrrolidone
2-Pyrrolidone is purified by contact with particulate calcium oxide for a sufficient time at elevated temperatures followed by distilling and condensing the purified 2-pyrrolidone....
06/30/1981
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