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| Number | Title | Issue Date |
| 7402720 | Distillation process for removal of methyl acetylene and/or propadiene from an olefin stream The present invention provides a process for removing methyl acetylene and/or propadiene from a propylene stream and/or a butylene stream by two step fractionation. Methyl acetylene and/or propadiene avoids the use of a hydrogenation reactor and makes the methyl ace... | 07/22/2008 |
| 7371309 | Purification of difluoromethane by extractive distillation The present invention provides extractive distillation processes for removing difluoromethane (HFC-32) from a mixture comprising HFC-32 and at least one of chlorodifluoromethane (CFC-12), 1,1,1-trifluoroethane (HFC-143a), chloropentafluoroethane (CFC-115), and penta... | 05/13/2008 |
| 7234691 | Radial-crossflow distillation trays for divided wall column applications An assembly of trays in a divided wall column having an inner column wall, a dividing wall, and an interior space includes: a first tray having at least one radial downcomer adjacent the dividing wall and extending radially toward the inner column wall a first subst... | 06/26/2007 |
| 7189311 | Purification of difluoromethane A method for separating difluoromethane from a mixture of difluoromethane and at least one impurity, the method involving extractively distilling the mixture using dichloromethane as an extractive agent to recover a product stream of purified difluoromethane having ... | 03/13/2007 |
| 7037412 | Method for preparing deodorized N-vinyl-2-pyrrolidone The invention provides a method for producing purified N-vinyl-2-pyrrolidone free of odorous components. The method is composed of distilling with a distillation column a liquid, which is formed by adding to an odorous components-containing liquid having a N-vinyl-2... | 05/02/2006 |
| 6984293 | Azeotropic distillation of cyclic esters of hydroxy organic acids Cyclic esters of hydroxy organic acids can be produced and recovered via azeotropic distillation. In certain embodiments cyclic esters, such as glycolide and lactide, can be produced from a fermentation broth or other feed stream that contains a hydroxy organic acid... | 01/10/2006 |
| 6982026 | Azeotropic distillation process for producing organic acids or organic acid amides Disclosed herein are methods for the recovery of at least one of an organic acid or an organic acid amide, such as a heat stable lactic acid or lactamide, from a feed stream which contains the organic acid and/or organic acid amide. The feed stream is mixed with at ... | 01/03/2006 |
| 6946060 | Purification of N,N-dimethylacetamide A method to purify N,N-dimethylacetamide (DMAc) from an aqueous solution containing acetic acid as a contaminant. Two fractional distillation columns are arranged in a series. The solution containing the contaminant is provided to the first column with a temperature... | 09/20/2005 |
| 6926810 | Process for obtaining an organic acid from an organic acid ammonium salt, an organic acid amide, or an alkylamine organic acid complex Disclosed herein are methods for the recovery of an organic acid, such as a heat stable lactic acid, from a feed stream which contains at least one of an organic acid amide, an organic acid ammonium salt, or an alkylamine-organic acid complex. The feed stream is mix... | 08/09/2005 |
| 6787001 | Method for distilling (meth) acrylic acid solution A method for distilling a raw material liquid containing (meth)acrylic acid substantially free from azeotropic solvents, collected with a collection agent from a mixed gas obtained by gas phase catalytic oxidation reactions which includes feeding to a distillation c... | 09/07/2004 |
| 6736941 | Process for purifying propylene oxide A process is described for purifying propylene oxide, which includes the step of distilling propylene oxide containing impurities in the presence of a hydrocarbon having 5 carbon atoms or less. According to the present invention, a process is provided for purifying ... | 05/18/2004 |
| 6679975 | Process for recovering the methanol contained in a liquid hydrocarbon feed The present invention aims to isolate the azeotropes formed in a distillation column (B1) by methanol, propane and butane. The azeotropes are then liquefied in heat exchanger (E2) and mixed in contactor (M1) with water in order to dissolve the methanol in... | 01/20/2004 |
| 6582565 | Recovery of 3,4-epoxy-1-butene by extractive distillation Disclosed is a process for the recovery and purification of 3,4-epoxy-1-butene (epoxybutene) from mixtures comprising epoxybutene and aliphatic and aromatic hydrocarbons containing five to seven carbon atoms having boiling points between about 20° C. and... | 06/24/2003 |
| 6500311 | Propylene oxide purification A mixture of propylene oxide and methanol is separated by liquid/liquid extraction using water and a hydrocarbon such as n-octane as extractive solvents.... | 12/31/2002 |
| 6461481 | Process for removing water from organoborane compounds A method of removing water from wet organoborane by dissolving the wet organoborane in an organic solvent in which water is incompletely soluble, decanting any insoluble water, and distilling the organic phase to remove water which may be contained therei... | 10/08/2002 |
| 6458249 | Process for purifying perfluorinated products Nitrogen trifluoride (NF3) containing less than 10 parts-per-million molar impurities, e.g., tetrafluoromethane (PFC-14), is disclosed. Azeotropic and extractive distillation processes using entraining agents for separating NF3 and P... | 10/01/2002 |
| 6444096 | Process for the recovery and purification of cyclobutanone A process for the recovery and purification of cyclobutanone from a crude product mixture obtained from an oxidation product mixture resulting from the oxidation of cyclobutanol to cyclobutanone in the presence of water. The process provides for the recov... | 09/03/2002 |
| 6383343 | Separation of components from methanol mixtures by extractive distillation A method of separating methanol and acetone, and methanol and methyl acetate involves distilling a mixture of the components by an extractive distillation process in the presence of an extractive distillation solvent. The extractive distillation solvent m... | 05/07/2002 |
| 6375807 | Separation of ethanol mixtures by extractive distillation A method of separating ethanol and ethyl acetate, and ethanol and water involves distilling a mixture of the components by an extractive distillation process in the presence of an extractive distillation solvent. The extractive distillation solvent may be... | 04/23/2002 |
| 6352618 | Modular solvent recovery device A process is disclosed for manufacturing a concentrated residue from a photopolymer fluid which includes photopolymer and photopolymer solvent. The photopolymer fluid may be derived by chemically etching a photopolymer layer of a printing plate with a sol... | 03/05/2002 |
| 6340414 | Process for the recovery of perfluorinated sulphonic acids from spent acid Process for the recovery of fluorinated sulphonic acid including the step of subjecting the spent acid to heat treatment with stepwise or continuously increasing temperature, withdrawing at least two fractions during the heat treatment; and recovering the... | 01/22/2002 |
| 6299736 | Process for recovering γ-butyrolactone from a mixture of heavy organics Gamma-Butyrolactone (GBL) is recovered from a mixture containing GBL and other heavy organics by a process of azeotropic distillation in the presence of a C8-C 10 hydrocarbon as an azeotroping agent, wherein an azeotrope of GBL and t... | 10/09/2001 |
| 6179967 | Purification process of pentrafluoroethane A purification process of pentafluoroethane from a crude pentafluoroethane containing chloropentafluoroethane as a by-product by extractive distillation using an extracting reagent having a standard boiling point of from -10° C. to 100° C. and being sel... | 01/30/2001 |
| 6166270 | Extractive distillation separation High purity tertiary butyl alcohol is obtained from mixtures comprised of tertiary butyl alcohol and tertiary butyl acetate by extractive distillation using a hydrocarbon extractive solvent such as decane.... | 12/26/2000 |
| 6120652 | Method for purifying crude 1,1,1,3,3-pentafluoropropane The invention relates to a method for purifying a crude 1,1,1,3,3-pentafluoropropane (HFC-245fa) containing HFC-245fa and 1-chloro-3,3,3-trifluoro-trans-1-propene (HCFC-1233zd(t)), by distillation. This method is characterized in that the distillation is ... | 09/19/2000 |
| 6066238 | Hydrocarbon separation A process for the separation of propylene from an input stream of C3 hydrocarbons containing propylene and methyl acetylene and/or propadiene and, optionally, C4 and/or higher hydrocarbons is described. The process includes subjecting the input stream to ... | 05/23/2000 |
| 6042697 | Separation of 9,11-Diene C18 fatty acid from 10,12-Diene C18 fatty acid by azeotropic distillation 9,11- Diene C18 fatty acid cannot be separated from 10,12-Diene C18 fatty acid by conventional rectification because of the proximity of their boiling points. 9,11-Diene C18 fatty acid can be readily separated from 10,12-Diene fatty acid by azeotropic dis... | 03/28/2000 |
| 6039846 | Separation of 3-methyl-2-pentenal from n-butanol by azeotropic distillation 3-Methyl-2-pentenal cannot be separated from 1-butanol by conventional rectification because of the proximity of their boiling points. 3-methyl-2-pentenal can be readily separated from n-butanol by azeotropic distillation. Effective agents are dimethoxyme... | 03/21/2000 |
| 6033530 | Continuous distillation of thermolabile monomers A process for the continuous distillation of thermolabile monomers under reduced pressure in a column includes feeding the thermolabile monomers in vapor or liquid form to the column, introducing an inert distillation aid which forms a heteroazeotrope with the... | 03/07/2000 |
| 6024841 | Separation of 2-methyl-1-butanol and 3-methyl-1-butanol from 1-pentanol by extractive distillation 2-Methyl-1-butanol and 3-methyl-1-butanol are difficult to separate from 1 pentanol by conventional distillation or rectification because of the proximity of their boiling points. 2-Methyl-1-butanol and 3-methyl-1-butanol can be easily separated from 1-pe... | 02/15/2000 |
| 5993610 | Separation of ethyl acetate from ethanol by azeotropic distillation Ethyl acetate cannot be separated from ethanol by distillation or rectification because of the closeness of their boiling points. Ethyl acetate is readily separated from ethanol by azeotropic distillation. Effective agents are ethyl ether, methyl formate ... | 11/30/1999 |
| 5964987 | Neutral oil removal from natural cresylic acid mixtures Natural cresylic acid is processed to remove neutral oil impurities by countercurrent liquid/liquid extraction using a heavy phase solvent of a mixture of glycerol and another polyhydric alcohol, preferably triethylene glycol. The light phase solvent is a... | 10/12/1999 |
| 5922175 | Purification of chlorotetraflouroethane by extractive distillation A process for the purification of 1-chloro-1,2,2,2-tetrafluoroethane (F124) containing 1,2-dichlorotetrafluoroethane (F114) and/or 1,1-dichlorotetrafluoroethane (F114a). The F124 to be purified is subjected to extractive distillation, the extractant being... | 07/13/1999 |
| 5908538 | Separation of T-amyl alcohol from 2- methyl-1 -propanol azeotropic distillation 2-Methyl-1-propanol cannot be separated from t-amyl alcohol by distillation or rectification because of the closeness of their boiling points. 2-Methyl-1-propanol is readily separated from t-amyl alcohol by azeotropic distillation. Effective agents are bu... | 06/01/1999 |
| 5904815 | Separation of t-amyl alcohol from n-butanol by azeotropic distillation t-Amyl alcohol cannot be separated from n-butanol by distillation or rectification because of the closeness of their boiling points. t-Amyl alcohol is readily separated from n-butanol by azeotropic distillation. Effective agents are propyl acetate, tetrah... | 05/18/1999 |
| 5897750 | Separation of acetone from isopropanol-water mixtures by extractive distillation Acetone cannot be separated from a mixture of isopropanol and water because of the closeness of their boiling points. Acetone can be easily separated from isopropanol and water by extractive distillation. Effective extractive agents are 1-nitropropane, 3-... | 04/27/1999 |
| 5882485 | Process for the separation of dimethyl ether and chloromethane in mixtures A process for the separation of dimethyl ether and chloromethane in mixtures A process for the separation of dimethyl ether and chloromethane in mixtures by two distillation steps. In the first step, the mixture is subjected to an extractive distillation ... | 03/16/1999 |
| 5879517 | Method for separating 2-butanol from t-amyl alcohol using certain organic compounds as the agent in extractive distillation 2-Butanol cannot be sparated from t-amyl alcohol by distillation or rectification because of the closeness of their boiling points. 2-Butanol is readily separated from t-amyl alcohol by extractive distillation. Effective agents are butyl ether, benzyl ace... | 03/09/1999 |
| 5876569 | Separation of methyl ethyl ketone from ethanol by extractive distillation Methyl ethyl ketone cannot be separated from ethanol by distillation or rectification because of the closeness of their boiling points. Methyl ethyl ketone is readily separated from ethanol by extractive distillation. Effective agents are methyl benzoate,... | 03/02/1999 |
| 5868907 | Separation of methyl ethyl ketone from ethanol by azeotropic distillation Methyl ethyl ketone cannot be separated from ethanol by distillation or rectification because of the closeness of their boiling points. Methyl ethyl ketone is readily separated from ethanol by azeotropic distillation. Effective agents are amyl acetate, me... | 02/09/1999 |
