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Class 568/383 - Processes


Subclass of Class 568 - Organic compounds -- part of the class 532-570 series
Definition: Processes which are directed to the preparation, purification,
No. of patents: 57
Last issue date: 02/09/2010


1    
NumberTitleIssue Date
7659430Method for separating hydrogen chloride and phosgene
The invention relates to a process for separating hydrogen chloride and phosgene, which comprises bringing a mixture of hydrogen chloride and phosgene into contact with an ionic liquid in which at least part of the hydrogen chloride is dissolved in a step a) and the...
02/09/2010
7416645Continuous process for recovering acetone from a waste stream resulting from acetone purification
The present invention provides a continuous process for recovering acetone from a waste stream from an acetone purification stage. The waste stream contains mesityl oxide and optionally acetone. The process for recovering acetone includes separating the waste stream...
08/26/2008
7314960Catalytic synthesis of oxygenate from alcohol
The present invention discloses a method for catalytic synthesis of oxygenate from alcohol. At first, a feeding material comprising at least one alcohol is provided. Next, a copper-containing catalyst is provided and the catalyst further comprises at least one metal...
01/01/2008
7304185Process for production of carbonyl compounds
There is provided a process for the production of carbonyl compounds, characterized by reacting a diol represented by the formula (1); wherein R1, R2, R3 and R4 are the...
12/04/2007
7176177Aromas and aroma compositions containing 4,8-dimethyl-3,7-nonadien-2-one, and a method for the production thereof
4,8-dimethyl-3,7-nonadien-2-one has aromatizing properties and increases the extendibility and intensity of the aroma when used in an aroma composition. ...
02/13/2007
7166752Decomposition of cumene oxidation product
A process for decomposing a cumene oxidation product mixture containing cumene hydroperoxide (CHP) and dimethylphenyl carbinol (DMPC) to produce phenol, acetone and alpha-methyl styrene (AMS) with enhanced safety of operation and reduced by-product formation which c...
01/23/2007
7166753Process for production of hydrogen and carbonyl compounds by reacting sub- or super-critical water with alcohols
A process for producing a carbonyl compound involves allowing water to undergo phase transition to a supercritical or subcritical state in the presence of an alcohol compound so as to produce/generate water-derived hydrogen and at the same time convert the alcohol c...
01/23/2007
7034193Method for purifying spent acid
A method for purifying a spent acid catalyst from an acid catalyzed chemical reaction that generates a mixture of a product, spent add and tar, includes the steps of separating the mixture of product, spent acid, and tar into a product fraction and a spent acid frac...
04/25/2006
6818799Process for removing tar from spent acid
There is a process for removing by-product tar during the manufacture of isopropyl alcohol. The process comprises the following: a) reacting propylene with concentrated sulfuric acid and water to form isopropyl alcohol and a spent acid having a by-product tar; b) ca...
11/16/2004
6780812Chiral lead catalyst and method of asymmetric aldol reaction
A novel chiral lead catalyst comprising a lead compound of the following formula: Pb(ORf)2 (wherein Rf represents a fluorine-containing alkylsulfonyl group) and a chiral crown ether compound hav...
08/24/2004
6759023Method for making a hydrazine by hydrolysing an azine
The invention relates to a process for manufacturing hydrazine by hydrolyzing an azine, in which the heat required for the reaction and the separation by distillation of the components is partly provided by injecting vaporized water. ...
07/06/2004
6576798Method and system for purifying cumene hydroperoxide cleavage products
A system for purifying a cumene hydroperoxide cleavage product mixture comprises a cumene hydroperoxide cleavage product mixture feed containing impurities in fluid communication with an aqueous alkaline solution feed; the cumene hydroperoxide cleavage pr...
06/10/2003
6573408System and method for purifying cumene hydroperoxide cleavage products
A system for purifying a cumene hydroperoxide cleavage product mixture comprises a cumene hydroperoxide cleavage product mixture feed containing impurities in fluid communication with an aqueous alkaline solution feed; the cumene hydroperoxide cleavage pr...
06/03/2003
6555715Conversion of light paraffins to oxygenates or olefins using an imide promoter
A process has been developed for oxygenating linear C2 to C6 alkanes to ketones or aldehydes. The process involves reacting the alkanes with oxygen in the presence of a catalyst comprising an imide promoter and a metal co-catalyst. A...
04/29/2003
6517798Method for preparing hydrazine hydrate
The invention concerns a method for making hydrazine hydrate which consists in hydrolyzing methyl ethyl ketone azine to obtain hydrazine hydrate and methyl ethyl ketone, characterised in that it consists in purging heterocyclic compounds of the pyrazoline...
02/11/2003
6479710Method of catalyzing a gas phase reaction using an acid-base catalyst composed of vanadium pentoxide hydrate
A solid acid-base catalyst contains vanadium pentoxide hydrate. Moreover, it is preferable that the vanadium pentoxide hydrate in the solid acid-base catalyst has a composition which is represented by the following general equation (1): V2 O
11/12/2002
6380437Process for the preparation of unsaturated 4,5-allene ketones, 3,5-diene ketones and the corresponding saturated ketones
Process for the preparation of unsaturated 4,5-allene ketones by reaction of tertiary propargyl alcohols with alkenyl alkyl ethers or ketals in the presence of aliphatic sulfonic acids or sulfonic acid salts....
04/30/2002
6376719Process for the preparation of alkaline earth metal salts of ଲ-diketo compounds
An alkaline earth metal salt of ଲ-diketo compound is produced using 1 mol of a powdery alkaline earth metal compound and 2.04 mol or more of an aliphatic ଲ-diketo compound. The reaction may be carried out while supplying both components to a r...
04/23/2002
6376718Dehydrogenation of alkylene glycol ethers to ether ketones and aldehydes
A catalytic dehydrogenation of alkylene glycol ether to ether ketone or aldehyde is disclosed. The dehydrogenation is performed with copper chromite catalyst and at least 5 wt % of water based on alkylene glycol ether. It has been found that the selectivi...
04/23/2002
6359179Direct carbonylation of paraffins using solid strong acid catalyst
A process for the direct carbonylation of saturated hydrocarbons has been developed. The process involves contacting the saturated hydrocarbons, which contain at least one primary, secondary or tertiary carbon atom, with carbon monoxide in the presence of...
03/19/2002
6340776Process for producing 1,1,1-trifluoroacetone
A process for producing 1,1,1-trifluoroacetone includes the step of conducting a hydrogenolysis of a halogenated trifluoroacetone, which is represented by the general formula (1), by a hydrogen gas in the presence of a catalyst containing a transition met...
01/22/2002
6329554Continuous preparation of unsaturated ketones
Process for the continuous preparation of unsaturated ketones of the formula I ##STR1## where the dashed line can be an additional C--C bond, R1 is an alkyl, and R2 is an aliphatic hydrocarbon having from 1 to 37 carbons, a cycl...
12/11/2001
6310258Process for preparing 1,3-diketones
The invention provides a process for preparing 1,3-diketones by rearrangement of the isomeric enol ester in a tube reactor comprising a heated portion and an unheated insulated portion which can optionally be provided with cooling means. The unheated port...
10/30/2001
6300524Process for preparing higher unsaturated ketones
The present invention relates to an improved process for preparing higher unsaturated ketones by reacting the corresponding ଱,ଲ-unsaturated alcohols with alkyl acetoacetates in a Carroll reaction , in a reactor system with fitted fractionation...
10/09/2001
6300523Noncatalytic organic synthesis using supercritical water
This invention is intended to provide a method for producing pinacoline by means of pinacol rearrangement in supercritical water, which affords an extremely high reaction rate without the addition of high concentrations of acid, and this invention is dire...
10/09/2001
6232506Process for producing 6-methyl-3-hepten-2-one and 6-methyl-2-heptanone analogues, and process for producing phytone or isophytol
Provided are a process for producing 6-methyl-3-hepten-2-one by cross aldol condensation carried out while each continuously adding to acetone, isovaleraldehyde and an aqueous alkali containing an alkaline substance; a process for producing a 6-methyl-2-h...
05/15/2001
6232505Methoxyacetone preparation
A process for making methoxyacetone is disclosed. The process comprises oxidizing 1-methoxy-2-propanol in the liquid phase using aqueous hydrogen peroxide and a Group 8-10 transition metal catalyst. The process gives high alcohol conversions (>95%) and go...
05/15/2001
6211412Synthesis of epothilones
Commercially feasible methods for synthesizing various epothilones precursors needed for the preparation of final epothilones are provided, including techniques for the synthesis of epothilone segment C using a stereoselective Noyori-type reduction, and t...
04/03/2001
6165352Process for dehydrogenating hydrocarbons and oxygenated hydrocarbons
A continuous process for the dehydrogenation of a hydrocarbon and/or oxygenated hydrocarbon feed, comprising contacting the hydrocarbon and/or oxygenated hydrocarbon feed with a dehydrogenation catalyst at elevated temperature in a reaction zone character...
12/26/2000
6072087Method for producing carbonyl compounds
The present invention relates to a process for the preparation of carbonyl compounds of the formula ##STR1## in which R1 denotes a hydrogen atom or an alkyl radical containing from 1 to 3 carbon atoms, R2 denotes a hydrogen atom...
06/06/2000
6051741Preparation of γ,δ-unsaturated ketones by the Carroll reaction, novel catalysts therefor and the preparation thereof
A process for preparing γ,δ-unsaturated ketones of the general formula I ##STR1## by reacting an allyl alcohol of the general formula II ##STR2## in which R1 is H or a hydrocarbon radical having 1 to 20 carbon atoms, with diket...
04/18/2000
6049010Method of preparing 3-(3-methyl-2-buten-1-yl)-2,4-pentanedione and related dicarbonyl compounds
A method for preparation of a dicarbonyl compound of the following formula ##STR1## by reacting a conjugated alkadiene compound of the formula ##STR2## with a 1,3-dicarbonyl compound of the formula ##STR3## in the presence of an acid cataly...
04/11/2000
6025530Phenol tar cracking process
The present invention relates generally to a method for treating phenol tar, and, more particularly to a method for separating valuable products from phenol tar by treating the tar with steam....
02/15/2000
5936129Process for making sterically-hindered ଲ-diketones
A process for making a sterically-hindered beta-diketone involving: (a) providing a solution comprising: (i) an ester; (ii) a base; and (iii) a solvent; (b) adding a ketone selected from the group consisting of an aromatic ketone and a hindered aliphatic ...
08/10/1999
5929286Method for making hydrogen rich gas from hydrocarbon fuel
A method of forming a hydrogen rich gas from a source of hydrocarbon fuel in which the hydrocarbon fuel contacts a two-part catalyst comprising a dehydrogenation portion and an oxide-ion conducting portion at a temperature not less than about 400° C. for...
07/27/1999
5914013Selective thermal and photooxidation of hydrocarbons in zeolites by oxygen
A process for selective thermal oxidation or photooxidation of hydrocarbons adsorbed onto zeolite matrices. A highly selective thermal oxidation and photooxidation of unsubstituted or alkyl substituted alkanes, alkenes, aromatics and cycloalkyls in solven...
06/22/1999
5905174Method for producing 3,3-dichloro-1,1,1-triflouroacetone
The invention relates to a method for producing 3,3-dichloro-1,1,1-trifluoroacetone. This method includes a step of fluorinating pentachloroacetone by hydrogen fluoride in the presence of a fluorination catalyst. This fluorination may be conducted in a li...
05/18/1999
5874635Preparation of γ, δ-unsaturated ketones by the carroll reaction in cyclic carbonates or γ-lactones
A process for preparing γ,δ-unsaturated ketones by a) reacting vinylcarbinols or propargyl alcohols with alkyl acetoacetates or diketene and b) thermally rearranging the resulting acetoacetates in the presence or absence of an aluminum catalyst to γ,δ-unsa...
02/23/1999
5786515Synthesis of ଱-chloro or fluoro ketones
A simple, high yielding synthesis of a-chloro ketones is described, involving acylation of Grignard and organolithium reagents with N-methoxy-N-methylchloroacetamide. The efficiency of the process is further enhanced by recycling N,O-dimethylhydroxylamine...
07/28/1998
5744071Processes for preparing alkynyl ketones and precursors thereof
The present invention provides processes for making alkynyl ketones and precursors thereof, using less expensive reagents and/or hydrocarbon solvents and/or higher temperatures....
04/28/1998
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