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Class 564/497 - Purification or recovery


Subclass of Class 564 - Organic compounds -- part of the class 532-570 series
Definition: Processes directed to the purification, separation, or recovery
No. of patents: 137
Last issue date: 07/12/2011


1        
NumberTitleIssue Date
7977514Process for isolation of an organic amine
The invention relates to a process for the isolation of an organic amine from a composition comprising the organic amine and an acid, or a salt of the organic amine and the acid, wherein the process comprises steps wherein ammonia or hydrazine is added to the compos...
07/12/2011
7560594Method for producing triethanolamine
Method of producing triethanolamine where a phosphane or a compound which liberates a phosphane is added to the triethanolamine. ...
07/14/2009
7550632Methods of treating triethanolamine with acid components and basic components, and triethanolamine compositions containing the same
Methods for improving color properties of triethanolamine, and triethanolamine compositions treated thereby, are disclosed, wherein the methods comprise: (a) providing a composition comprising triethanolamine; and (b) contacting the composition with an acid componen...
06/23/2009
7425652Preparation of alkanolamines
Alkanolamine compositions are disclosed. The composition comprises an alkanolamine and hydroxylamine or hydrazine. Preferred alkanolamine includes diethanolamine, triethanolamine, and mixtures thereof. The composition of the invention has significantly reduced disco...
09/16/2008
7329354Purification of organic solvent fluids
A chemical distribution system having improved organic solvent fluid purity and consistency includes a vessel containing ion-exchange media positioned within a fluid flow pathway such that the organic solvent fluid passes through the ion-exchange media, thereby effe...
02/12/2008
7323600Process for improving the conversion of oxazolidones to alkanolamines
There is provided a regeneration process for converting oxazolidones such as hydroxypropyloxazolidone (HPOZD) to alkanolamines such as di-isopropanolamine (DIPA) and CO2. An amine stream containing HPOZD joins a stream that includes a caustic solution. Th...
01/29/2008
7271292Process for distillatively removing piperazine from an ethylenediamine-piperazine mixture
The invention relates to a process for continuously, distillatively removing piperazine from an ethylenediamine-piperazine mixture under pressure at elevated temperature, by discharging the ethylenediamine at the top and the piperazine at the bottom of a distillatio...
09/18/2007
7208632Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine
The invention relates to the field of separation by distillation of 6-aminocapronitrile (ACN) and hexamethylenediamine (HMD) from a mixture comprising ACN, HMD, tetrahydroazepine (THA), adiponitrile (ADN) and low boilers (LB). Also disclosed is a method for producin...
04/24/2007
7169268Color stabilization of amines
The present invention concerns a process for providing tertiary amine products which are color-stable, and have a greatly reduced tendency to take on color during their storage. According to the invention, an ethyleneamine derivative is added to the distillation pot...
01/30/2007
7164044Process for producing high purity trialkanolamine
A process for producing a high purity trialkanolamine excelling in hue and having an APHA of not more than 40, characterizing by including producing a mixed alkanolamine by the reaction of an alkylene oxide with ammonia; removing low-boiling substances from the mixe...
01/16/2007
7147757Method for separating an azepine derivative out of a mixture containing an amine an azepine derivative
The invention relates to a method for separating by distillation a portion or the entirety of an azeptine derivative (III), which is selected from the group consisting of aminohexylidene imine, tetrahydroazepine, hexylhexahydroazepine and of aminohexylhexahydroazepi...
12/12/2006
7029557Method for producing an aqueous hydroxylamine solution devoid of salt
The invention relates to a method for producing a highly pure, aqueous hydroxylamine solution by distilling an aqueous solution, devoid of salt, of a hydroxyl ammonium salt in a plate column comprising at least two mechanical plates. Said method is characterised in ...
04/18/2006
6986833Process for fractionating water-containing crude amine mixtures from amine synthesis
An amine-containing mixture containing one or more amines, water, low-boilers and optionally high-boilers is fractionated by a process having the steps (iii) and (iv) and optionally the steps (i), (ii) and (v): (i) a (first) low-boiler fraction is separ...
01/17/2006
6951960Method for removing impurities from solvent extraction solutions
A method for regenerating an amine extractant used for recovery of metals involves contacting a liquid organic phase containing an amine complexed with one or more metals with an aqueous solution substantially free of chloride ions to strip the one or more metals fr...
10/04/2005
6913674Process for fractionating water-containing crude amine mixtures from amine synthesis
A mixture containing one or more amines, water, low-boilers and high-boilers, is fractioned in a process wherein (i) low-boilers are separated from the mixture by distillation, (ii) high-boilers are separated from the mixture by distillatio...
07/05/2005
6887352Distillative method for separating hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine
A method for recovering hexamethylene diamine (HMD) from a mixture comprising HMD, 6-aminocapronitrile (ACN) tetrahydroazepine (THA), and adiponitrile (ADN) is disclosed. The method includes introducing the mixture into a first distillation column, separating...
05/03/2005
6846959Process for producing alkanolamines
A process for producing an alkanolamine includes supplying a reactive distillation apparatus having an inner contacting surface which simultaneously facilitates a reaction process and a distillation process, feeding a first reactant including an amine represented by...
01/25/2005
6821396Process for fractionating water-containing crude amine mixtures from amine synthesis
A mixture containing mixture one or more amines, water, low-boilers and high-boilers, is fractioned in a process wherein (i) low-boilers are separated from the mixture by distillation, (ii) high-boilers are separat...
11/23/2004
6818794Extraction of ketazine solutions
Process for extracting aqueous ketazine solutions which is carried out using an aqueous ketazine solution having a salt content of 5 to 27% by weight and an ammonia content of 0 to 28% by weight to extract at temperatures of 50 to 120° C., which is characterized in...
11/16/2004
6784320Amine recovery method and apparatus and decarbonation apparatus having same
In a decarbonation process for removing carbon dioxide from a carbon dioxide-containing gas with the use of an amine compound-containing absorbing solution, an amine compound accompanying a decarbonated exhaust gas is efficiently recovered in the following manner: A...
08/31/2004
6774270Method of removing hexafluoropropylene dimers
A method of removing hexafluoropropylene dimers (“HFP dimers”), dimer hydrides and other oligomers from a fluid is described. The method comprises heating the fluid to isomerize the HFP dimers to the thermodynamic isomer, and contacting the fluid with a tertiary...
08/10/2004
6774264Catalyst to improve the color stability of N,N-dialkylalkanolamines
This invention relates to an improvement in a process for effecting decolorization of an alkanolamine by subjecting the alkanolamine to hydrogenation in the presence of a hydrogenation catalyst. The improvement for removing color, by-products, or both from a dialkyl...
08/10/2004
6683217Process for manufacturing triethanolamine and product obtained
The present invention relates to a continuous process for the manufacture of triethanolamine (TEA) comprising, in succession: (i) a step of synthesizing the TEA by continuously bringing ammonia into contact with ethylene oxide under conditions allowing th...
01/27/2004
6599398Recovery of adiponitrile from a mixture of adiponitrile, aminocapronitrile and hexamethylenediamine
Process for the recovery of a purified adiponitrile (ADN) from a mixture of adiponitrile, aminocapronitrile and hexamethylenediamine, utilizing two sequential distillations: (1) a first distillation in which the mixture is distilled in a distillation colu...
07/29/2003
6573406High-purity alkanolamines and their production process
High-purity alkanolamines, whose iron content is less than 50 ppb, are provided. Said high-purity alkanolamines can be produced by covering with an alkanolamine-resistant material at least a part of the inner wall of equipment that contacts alkanolamines ...
06/03/2003
6515036Method of decomposing a polyurethane
A method of recovering a decomposition product from a polyurethane, the method comprising the steps of thermally decomposing a polyurethane into a liquid containing a polyol and a urea compound which is soluble in the polyol, and solids containing a urea ...
02/04/2003
6489373Method for decomposition and recovery of polyurethane resin
The present invention provides a method of recovering a polyamine compound and/or a polyol compound useful for starting materials of polyurethane resin in an industrially advantageous manner by first dissolving the polyurethane resin such as polyurethane ...
12/03/2002
6462230Method of and apparatus for decomposing wastes
A method of decomposing wastes containing target compounds having one or more of hydrolyzable bonds of ether bond, ester bond, amide bond and isocyanate bond wherein the method comprises continuously supplying the wastes in a molten state or liquid state ...
10/08/2002
6384216Purification of alkenyl compounds
A process for purifying alkenyl compounds having a divalent or trivalent heteroatom in the ଱-position relative to the double bond by distillation comprises carrying out at least two distillations in which the purified alkenyl compounds are obtained ...
05/07/2002
6353138Process for purifying aqueous tertiary amine and alkanolamine solutions
A process for the removal of primary and secondary amine and alkanolamine impurities from aqueous tertiary amine and alkanolamine solutions without affecting the tertiary amine and/or alkanolamine by treating these solutions with a monoaldehyde or dialdeh...
03/05/2002
6291715Process for the preparation of alkanolamines having improved color quality
Preparation of alkanolamines having improved color quality by treating the alkanolamine with hydrogen in the presence of a hydrogenation catalyst at elevated temperature, by using, as hydrogenation catalyst, a heterogeneous catalyst comprising Re, Ru, Rh,...
09/18/2001
6255529Method of and apparatus for decomposing wastes
A method of decomposing wastes containing target compounds having one or more of hydrolyzable bonds of ether bond, ester bond, amide bond and isocyanate bond wherein the method comprises continuously supplying the wastes in a molten state or liquid state ...
07/03/2001
6153799Method for producing highly pure aqueous hydroxylamine solutions
A very pure aqueous solution of free hydroxylamine is prepared by a process in which the dilute, aqueous hydroxylamine solution is concentrated in a column by removing hydroxylamine-containing vapors via a side take-off in the bottom of the column, and ve...
11/28/2000
6153784Removal of halides from halide-containing nitrile mixtures
Halides are removed from halide-containing nitrile mixtures by (a) thermally treating the halide-containing nitrile mixture, (b) subsequently adding a base to the thermally treated nitrile mixture and (c) subsequently separating off the base from the nitrile mixture. Am...
11/28/2000
6117948Process for producing aliphatic amine derivative
The present invention provides a process for easily producing an alkylene oxide adduct to an aliphatic amine compound which has a fully excellent color, is not turbid, and does not deteriorate in color even through long-term storage. That is, the present ...
09/12/2000
6111142Process for the preparation of an aminoalcohol
A process for the preparation of 3-amino-1,2-propanediol, commonly known as isoserinol, having an organic impurities content lower than 0.1% and an inorganic impurities content lower than 0.05%....
08/29/2000
6077976Process for recovery of aminoalcohols from aqueous solutions containing inorganic salts
A process for recovery of aminoalcohols from aqueous solutions containing inorganic salts is disclosed. The aqueous solution which contains aminoalcohols is then mixed with a base in order to increase the ph and the solution is then extracted with an alky...
06/20/2000
6054620Process for producing a tertiary amine having high quality
The present invention provides a process for producing a tertiary aliphatic amine having high quality having little non-amines such as esters and alcohols, which is less colored, and which can be converted into a derivative without turbidity. That is, the...
04/25/2000
6046362Recovery of amines from emulsions
The instant invention is directed to a method for recovering surface active amines from an emulsion comprising the salt of the amine comprising (a) contacting an emulsion layer or phase containing surface active amine salt with an acid selected from the g...
04/04/2000
5912387Amine heat stable salt neutralization having reduced solids
A process is disclosed for the neutralization of amine or alkanolamine heat stable salts with aqueous KOH or with alkali metal base, such as potassium hydroxide, sodium hydroxide, sodium carbonate, potassium carbonate, sodium bicarbonate or potassium bica...
06/15/1999
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