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Class 562/494 - Purification or recovery per se


Subclass of Class 562 - Organic compounds -- part of the class 532-570 series
Definition: Processes directed to the purification, separation, or recovery
No. of patents: 82
Last issue date: 01/05/2010


1      
NumberTitleIssue Date
7642374Process for producing 5-iodo-2-methylbenzoic acid
The present invention provides a process for producing 5-iodo-2-methylbenzoic acid through iodination of 2-methylbenzoic acid, the process including, as essential steps, a reaction step of iodinating 2-methylbenzoic acid in the presence of a microporous compound, io...
01/05/2010
7402694Process for removal of benzoic acid from an oxidizer purge stream
A process is disclosed that relates to the removal of impurities, specifically benzoic acid, from a mother liquor produced in the synthesis of carboxylic acid, typically terephthalic acid. ...
07/22/2008
7288322Self-adhesive, addition cross-linking silicone-rubber blends, method for their production, method for producing composite molded parts and use of the latter
Self-adhesive, addition cross-linking silicone-rubber blends which have good adhesion to substrates but which release from molds used to prepare molded parts from them. ...
10/30/2007
7282151Process for removal of impurities from mother liquor in the synthesis of carboxylic acid using pressure filtration
A process is disclosed that relates to the recovery of a metal catalyst from an oxidizer purge stream produced in the synthesis of carboxylic acid, typically terephthalic. More particularly, the process involves recovery of a metal catalyst from an oxidizer purge st...
10/16/2007
7253299Process for purifying n2-(1(s)-ethoxycarbonyl-3-phenylpropyl)-n6-thifluoroacetyl-l-lysine
A process for purifying N2-(1(S)-ethoxycarbonyl-3-phenylpropyl)-N6-trifluoroacetyl-L-lysine which comprises subjecting N2-(1(S)-ethoxycarbonyl-3-phenylpropyl)-N6-trifluoroacetyl-L-lysine contaminated with impurities to cry...
08/07/2007
6777213Isolation of carboxylic acids from fermentation broth
A process for recovering carboxylic acids from an aqueous mixture such as a fermentation broth using a solvent containing at least one olefin without the need for first removing the spent microorganism cells is provided. A co-solvent which increases the partition co...
08/17/2004
6660505Isolation of carboxylic acids from fermentation broth
A process for recovering carboxylic acids from an aqueous mixture such as a fermentation broth using a solvent containing at least one olefin without the need for first removing the spent microorganism cells is provided. A co-solvent which increases the p...
12/09/2003
6642412Process for producing a high purity aromatic polycarboxylic acid
A process for producing a high purity aromatic polycarboxylic acid by purifying a crude aromatic polycarboxylic acid in accordance with the steps of (I) forming an amine salt of an aromatic polycarboxylic acid from the crude polycarboxylic acid and an ami...
11/04/2003
6639104Process for the recovery of purified terephthalic acid (PTA)
A process for the preparation of purified terephthalic acid which comprises first introducing a liquid slurry containing crystalized terephthalic acid with impurities into a high pressure rotary filter, then filtering the slurry with the high pressure rot...
10/28/2003
6548695Process for producing isocoumarins and intermediates for the same
Provided is a process for producing an isocoumarin-3-yl-acetic acid derivative, characterized by reacting a homophthalic acid derivative represented by a formula: ##STR1## (wherein Rc, R2 and R are mainly protecting groups) with a ...
04/15/2003
6491795Process for recovering benzyl benzoate
High-purity benzyl benzoate is recovered by distilling the residue remaining after removal of unreacted toluene and benzoic acid from a reaction mixture produced by the oxidation of toluene by molecular oxygen in the presence of a metal catalyst thereby s...
12/10/2002
6455731Process for producing a high purity aromatic polycarboxylic acid
A process for producing a high purity aromatic polycarboxylic acid by purify a crude aromatic polycarboxylic acid in accordance with the steps of (I) forming an amine salt of an aromatic polycarboxylic acid from the crude polycarboxylic acid and an amine,...
09/24/2002
6441225Purification of aromatic diacids
A method is provided to produce dicarboxylic or tricarboxylic aromatic acid from salts of such acids, the method including the steps of providing an aqueous solution of a salt of a dicarboxylic or tricarboxylic aromatic acid, the aqueous solution having a...
08/27/2002
6437179Process for the preparation of fluorogenic phenolic compounds
A method is disclosed for preparing a fluorogenic phenolic compound with improved optical qualities for use in formulating a substrate solution for assay of peroxidase or peroxide activity. The method involves forming a solution under anoxic conditions wh...
08/20/2002
6437176Method for preparing aromatic carboxylic acids, aromatic aldehydes, and aromatic alcohols
An aromatic carboxylic acid, aromatic aldehyde, and aromatic alcohol are simultaneously and efficiently prepared by liquid phase oxidizing an aromatic compound represented by formula (I) with a gas containing molecular oxygen, in a presence of a catalyst ...
08/20/2002
6403828Method of refining crystalline material
This invention relates to a process for purifying crystalline substances by charging the feed crystals containing impurities in a solid state to the top of a tower-type continuous crystallizer equipped with an agitating device, bringing said solid feed cr...
06/11/2002
6399790Method for oxidation of xylene derivatives
Xylene derivatives, such as chloro-ortho-xylene, are oxidized in a solvent in the presence of at least one metal catalyst and optionally at least one promoter. The product comprises chlorophthalic acid or chlorophthalic anhydride....
06/04/2002
6344568Catalyst for gas phase partial oxidation
This invention relates to a method for producing a partially oxidized organic compound, e.g., an unsaturated aldehyde/carboxylic acid having three or more carbon atoms, or an organic acid anhydride/nitrile compound having four or more carbon atoms. This m...
02/05/2002
6342636Process for preparing optically active amines and optically active carboxylic acids, and intermediates for preparation
Disclosed is a process for preparing an optically active 1-aryl- or 2-aryl-alkylamines of formulas Ia, Ib and Ic with high optical purity and high yield. The process uses an optically active 1- or 2-naphthylglycolic acid of the general formula II as a res...
01/29/2002
6307091Trifluoro-substituted benzoic acid, esters thereof and processes for preparing the same
The present invention is to provided a trifluoro-substituted benzoic acid, an ester thereof, particularly 2,3,4-trifluoro-5-iodobenzonic acid, 2,3,4-trifluoro-5-trifluoromethylbenzonic acid, esters thereof, which are useful as a starting material for synt...
10/23/2001
6255525Process for preparing purified carboxylic acids
A process for preparing an aromatic carboxylic acid having improved purity comprising contacting at an elevated temperature and pressure a mixture comprising an impure aromatic carboxylic acid and a solvent in the presence of hydrogen gas with a carbon ca...
07/03/2001
6254779Treatment of effluent streams containing organic acids
An acidic organics-containing waste water stream (12) derived from for example plant for the production of an aromatic carboxylic acid such as terephthalic acid is treated to allow recovery of alkali and water for recycle to the production process. The tr...
07/03/2001
6248797Supercritical carbon dioxide extraction of contaminants from ion exchange resins
A method for extracting leachable contaminants from ion exchange resins comprises exposing the resin to supercritical carbon dioxide for a sufficient interval of time to allow at least a portion of the leachable contaminant to be solubilized by the superc...
06/19/2001
6211404Method of refining benzoic acid
This invention relates to a process for purifying benzoic acid continuously to a purity of 99.9% or more by introducing crystals of crude benzoic acid with a bulk density of 0.2 g/cm3 or more and an average particle diameter of 0.3 mm or more i...
04/03/2001
6160171Trifluoro-substituted benzoic acid, esters thereof, and process for producing the same
The present invention is to provide a trifluoro-substituted benzoic acid, an ester thereof, particularly 2,3,4-trifluoro-5-iodobenzoic acid, 2,3,4-trifluoro-5-trifluoromethylbenzoic acid, esters thereof, which are useful as a starting material for synthes...
12/12/2000
6093830Enantioselective resolution process for arylpropionic acid drugs from the racemic mixture
The invention relates to a novel non-catalytic enantioselective resolution process for the separation of enantiomer of arylpropionic acid drugs from the racemic mixture, which comprises dissolving the racemic mixture of the said drug an organic solvent, r...
07/25/2000
5994560Resolution of racemic mixtures using polymers containing chiral units
Described herein is a novel process to resolve a racemic compound into its optically active isomers without need for chemical transformation such as salt formation. The process advantageously utilizes polymers containing chiral moieties in their repeat un...
11/30/1999
5843863Process for improving flow characteristics of crystalline ibuprofen
A process for producing crystalline ibuprofen having a crystal habit characterized by a particle length larger than 75 microns average and a length to width aspect ratio of greater than about 4 to 1 to about 5 to 1. The process involves crystallizing ibup...
12/01/1998
5739383Resolution of racemic mixtures using polymers containing chiral units
Described herein is a novel process to resolve a racemic compound into its optically active isomers without need for chemical transformation such as salt formation. The process advantageously utilizes polymers containing chiral moieties in their repeat un...
04/14/1998
5543564Process for releasing acidic organic compounds from salts thereof by carbon dioxide
This invention embodies a process for releasing acidic organic compounds in high yield and good purity from aqueous solutions of their salts which comprises converting the salts by carbon dioxide to their corresponding free acidic organic compounds and me...
08/06/1996
5426215Process for converting [R(-)-2(3-benzoylphenyl)-propionic acid to the S(+) isomer]
Process for transforming (benzoyl-3-phenyl)-2-propionic-R(-) acid into an S(+) isomer through the action of a base either in situ during the splitting of racemic ketoprofen or on the crystallization mother liquor of a (benzoyl-3-phenyl)-2-propionic-S(+) a...
06/20/1995
5399707Selective precipitation of ଱-aryl carboxylic acid salts
A process is provided whereby S(+)-ibuprofen or R(-)-ibuprofen L-lysinate salt is produced by selective precipitation from a mixture containing enantiomers of ibuprofen and L-lysine. The quantity of L-lysine is not more than about a molar equivalent of th...
03/21/1995
5384413Process for the preparation of tetrafluorophthalic acid and/or tetrafluorophthalic anhydride
The present invention relates to a process for the preparation of tetrafluorophthalic acid and/or tetrafluorophthalic anhydride by reacting a compound of the formula ##STR1## in which X is a radical ##STR2## which is optionally mono- or pol...
01/24/1995
5364962Method for purification of a benzoic acid
The invention relates to a method for the purification of benzoic acid, which is obtainable through oxidation of the corresponding toluene derivative, by treating it with a --NH2 or --NHR containing component in which R represents a carbon cont...
11/15/1994
5352825Recovery of organic acid salts from impure process streams by addition of bases
This invention provides an improved method for recovering an organic acid as a salt from various process streams by addition of a crystallizing base to a concentrated solution of neutralized organic acid. The addition of such a base causes crystallization...
10/04/1994
5352823Process for improving flow characteristics of crystalline ibuprofen
A process for producing crystalline ibuprofen having a crystal habit characterized by a particle length larger than 75 microns average and a length to width aspect ratio of greater than about 4 to 1 to about 5 to 1. The process involves crystallizing ibup...
10/04/1994
5336806Purification of 2,4,5-trifluorobenzoic acid
Disclosed is a process for isolating and purifying 2,4,5-trifluorobenzoic acid from a solution in a decarboxylating solvent such as NMP. The solution is neutralized with a hydroxide. This results in the formation of a salt of the 2,4,5-trifluorobenzoic ac...
08/09/1994
5324750Compositions and methods for drug delivery and chromatography
Cyclodextrin derivatives and inclusion complexes having increased solubility and stability are provided. Cyclodextrin derivatives include amino and other modified cyclodextrins, and linked cyclodextrins. Inclusion complexes comprising the foregoing cyclod...
06/28/1994
5254714Hydrogenation of aromatic-substituted olefins using organoruthenium catalyst
A process is disclosed for the enantioselective hydrogenation of olefins of the formula: ##STR1## where R is hydrogen or C1 to C6 linear or branched alkyl, Z is ##STR2## where R' is hydrogen or C1 to C6
10/19/1993
5233085Preparation of 2,4,5-trifluorobenzoic acid by decarboxylation of 3,4,6-trifluorophthalic acid
3,4,6-Trifluorophthalic acid may be decarboxylated in a controlled manner to form 2,4,5-trifluorobenzoic acid by heating the phthalic acid in a dipolar aprotic solvent in the absence of any catalyst....
08/03/1993
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