...that while attempting to develop a super strong glue, 3M employee Spencer Silver accidentally developed a glue that was so weak it would barely hold two pieces of paper together? However, his colleague Art Fry needed the glue. Fry sang with his church choir and marked the pages of his hymnal with small scraps of paper that often fell out. He used Silver's glue to hold the papers in place. Today we call this invention Post-it Notes.
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| Number | Title | Issue Date |
| 6916368 | Curable film-forming composition exhibiting improved scratch resistance A curable film-forming composition is provided that on curing produces a coating, comprising in a medium (i) 10 to 90 percent by weight based on the total weight of resin solids in the film-forming composition of a crosslinking agent; (ii) 10 to 90 percent by weight... | 07/12/2005 |
| 6790419 | Purification of gaseous inorganic halide The present invention provides an apparatus and method for the purification of gaseous inorganic halides utilizing a reactive metal and molecular sieves to remove impurities. ... | 09/14/2004 |
| 6238636 | Process and systems for purification of boron trichloride Processes are disclosed for increasing the condensed phase production of BCl3 comprising less than about 10 ppm phosgene, less than 10 ppm chlorine, and less than 10 ppm HCl. In one embodiment the process comprises injecting an inert gas into a... | 05/29/2001 |
| 5993766 | Gas source and dispensing system A system for the storage and delivery of a sorbable fluid, comprising a storage and dispensing vessel containing a sorbent material having sorptive affinity for the sorbable fluid, and from which the fluid is desorbable by pressure-mediated and/or thermal... | 11/30/1999 |
| 5938969 | Fire suppressant powder A fire suppressant powder with particle sizes less than 5 μm is made by a chemical reaction between a gas or vapour of a first material and a vapour or an aerosol of a second material. For example an aerosol of sodium hydroxide droplets may be reacted wi... | 08/17/1999 |
| 5489673 | Iodinated borane cage molecules as X-ray contrast media Highly iodinated borane and carborane cage molecules, having from 60% to 90% w/w iodine, are disclosed as new and useful X-ray contrast media when combined with a pharmaceutically acceptable carrier. The inclusion of appropriate functional group substitue... | 02/06/1996 |
| 5256394 | Radiological imaging method, and contrast media reagents therefor A method of imaging a corporeal situs by radiological techniques, comprising delivery to the corporeal situs of an imagingly effectively amount of a physiologically acceptable composition comprising a boron reagent. A variety of illustrative boron reagent... | 10/26/1993 |
| 5053365 | Method for the low temperature preparation of amorphous boron nitride using alkali metal and haloborazines The invention relates to an energy efficient method for the production of boron nitride materials at temperatures of from about 100 degrees to about 230 degrees Centigrade. The boron nitride materials produced by the present invention are carbon-free and ... | 10/01/1991 |
| 4971777 | Process for the removal of acid components and nitrogen oxides from the waste gases of industrial furnaces The process removes acid components including sulfur oxides and nitrogen oxides from the exhaust gases of industrial furnaces and includes oxidizing the nitrogen oxide contained in the exhaust gases with the oxygen contained in the exhaust gases at a exha... | 11/20/1990 |
| 4957722 | Production of partially calcined carbonaceous reductant using steam A process for producing chlorides by the chlorination of a material selected from the group consisting of aluminous materials and metal and metalloid oxides in the presence of a reductant. The method comprises calcining a carbonaceous material with added ... | 09/18/1990 |
| 4863706 | Process for producing zirconium sols and gels, and process for producing zirconia using the same A process for producing acidic boratozirconium chloride sols which comprises: reacting a zirconium compound with a boron compound in molar ratios of B/Zr of 0.3-1.2 together with a compound of a metal M, the metal M being selected from the group consistin... | 09/05/1989 |
| 4576636 | Process for beneficiating oxidic ores A process for the beneficiation of an iron-containing material is carried out by first chlorinating the iron-containing material. Oxidation of ferrous chloride in the effluent gas from the chlorination is carried out under controlled conditions of oxygen ... | 03/18/1986 |
| 4529707 | Detection of boron impurities in chlorosilanes A method for preparing a chlorosilane sample to enable colorimetric detection of the presence of minute amounts of boron impurities is provided. Detection of boron impurities below five parts per billion is contemplated.... | 07/16/1985 |
| 4528164 | Concurrent production of anhydrous non-metal and metalloid halides and ceramic materials with the aid of magnesium halide Molten alkaline earth metal halides are used to convert highly stable oxides into the corresponding anhydrous halides. Usually a third reactant, such as silica, is added in order to bind the basic oxide thus formed. The solid oxide compounds (e.g. silicat... | 07/09/1985 |
| 4490344 | Production process of silicon tetrachloride Silicon tetrachloride is effectively and efficiently produced at a relatively low temperature and at a high yield by (1) feeding a mixture of a silicon dioxide containing substance and carbon to the top of a reactor in which a reaction mixture forms a dow... | 12/25/1984 |
| 4414187 | Preparation of metal phosphates by a reaction using boron phosphate Metallic phosphates are prepared by heating mixtures of BPO4 and a metallic oxide or salt.... | 11/08/1983 |
| 4327062 | Process for producing chloride of elements of Group III, IV or V of Periodic Table The chlorides of elements of Groups III, IV and V of the Periodic Table, such as, boron trichloride, silicon tetrachloride, zirconium tetrachloride and vanadium tetrachloride are prepared by heating activated carbon particles having a supported aqueous so... | 04/27/1982 |
| 4239738 | Method for producing boron trichloride Boron trichloride is prepared by free radical liquid phase chlorination of borate ester, e.g., trimethylborate, at temperatures of between about 0° C. and 100° C., in the presence of an inert liquid organic solvent, e.g., carbon tetrachloride. The react... | 12/16/1980 |
| 4238465 | Removal of phosgene from boron trichloride Boron trichloride containing minor amounts of phosgene as an impurity is purified by contacting a vaporous stream thereof and at least a stoichiometric amount of hydrogen, based on the phosgene impurity, with a substantially metal-free carbon catalyst und... | 12/09/1980 |
| 4213948 | Preparation of boron trichloride Boron trichloride is prepared by free-radical chlorination of liquid borate ester, e.g., trimethyl borate, at temperatures of between about 20° C. and 100° C. Color bodies which form and accumulate in the liquid reaction mixture are removed by extractin... | 07/22/1980 |
| 4210631 | Preparation of boron trichloride Boron trichloride is prepared in substantially stoichiometric quantities by free-radical chlorination of borate ester, e.g., trimethyl borate, at temperatures of between about 20° C. and 100° C., more preferably between about 40° C. and about 90° C. T... | 07/01/1980 |
| 4172115 | Preparation and use of sulfur tetrachloride derivatives of the formula [SA3+.MXn+1.sup.- ] Sulfur tetrachloride derivatives are prepared by reacting suitable sulfur-containing compounds in hydrogen fluoride with a gas containing molecular chlorine in the presence of one or more acidic halides. Such derivatives can be used to remove water from i... | 10/23/1979 |
| 4125590 | Method for manufacturing boron trichloride This invention relates to the manufacture of boron trichloride from a molten salt bath comprising a naturally occurring boric acid salt or other boron-containing ore, carbon and chlorine gas. In accordance with the process of this invention, boron trichloride ... | 11/14/1978 |
| 4089931 | Purification of boron nitride Boron nitride (BN) is freed of boric oxide without increasing its electroconductivity by heating the BN under vacuum to evaporate the boric oxide and chlorinating the BN at a temperature sufficient to remove any elemental boron as boron trichloride.... | 05/16/1978 |
| 4024221 | Low temperature method of producing boron trichloride in a molten bath A low temperature method of producing boron trichloride comprises reacting an oxide of boron and a reducto-chlorinating agent in a molten bath comprising a combination of metal chlorides having a melting point of not more than 600° C, to form boron trich... | 05/17/1977 |
| 3996120 | Laser-induced photochemical enrichment of boron isotopes A boron trichloride starting material containing both boron-10 isotopes and oron-11 isotopes is selectively enriched in one or the other of these isotopes by a laser-induced photochemical method involving the reaction of laser-excited boron trichloride wit... | 12/07/1976 |