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Attorney: Tao; James F., Fuerle; Richard D.


Number of patents: 32
Last date: July 28, 1992

NumberTitleIssue Date
5133947Hydrous trivalent chromium oxide/carbon particles and method of making the same
Disclosed is a method of making particle which comprise hydrous trivalent chromium oxide having the empirical formula CrO2 H intimately associated with a pulverulent carbonaceous substrate. A composition is formed which comprises an aqueous sol...
07/28/1992
5130490Purification of 3,5-diaminobenzotrifluoride by selective precipitation of the hydrochloride salt
3,5-Diaminobenzotrifluoride can be readily separated from 4-chloro-3,5-diaminobenzotrifluoride by the addition of hydrogen chloride. 3,5-Diaminobenzotrifluoride forms hydrochloride salt, while 4-chloro-3,5-diaminobenzotrifluoride does so much less readily...
07/14/1992
5122238Efficient electrolytic method of making chromic acid from sodium bichromate
Disclosed is a method of making chromic acid by electrolyzing an aqueous solution of sodium bichromate until the sodium bichromate is converted to chromic acid at a bichromate percent conversion of about 1 to about 48.4. Sulfuric Acid is then added to the...
06/16/1992
5108722Sulfate removal from chlorate liquor
Disclosed is a method of removing sulfate ion from an aqueous sodium chlorate liquor. A crystallization temperature is selected between about -15° and about 0° C. and the maximum concentration of sodium chlorate that is soluble in the liquor at that tem...
04/28/1992
5104946Solutions of polyimidesiloxanes in butyrolactone
Disclosed is a solution in butyrolactone of a diglyme-insoluble polyimidesiloxane. The polyimidesiloxane is the reaction product of a dianhydride selected from the group consisting of 3,3',4,4'-benzophenone tetracarboxylic acid dianhydride, 3,3',4,4'-oxyd...
04/14/1992
5104500Ion exchange removal of impurities from chlorate process liquors
Disclosed is an improved method of operating a sodium chlorate crystal production system where a brine stream is electrolyzed to form sodium chlorate, the sodium chlorate is crystallized in a crystallizer, and the mother liquor from a crystallizer is recy...
04/14/1992
5098593Mixtures of perchloroethylene and monochlorotoluene
Disclosed is a composition of about 25 to about 85 wt % perchloroethylene and about 15 to about 75 wt % monochlorotoluene. When the composition contains at least about 30 wt % perchloroethylene it does not display a flash point....
03/24/1992
5084261Recovery and utilization of gypstack leachate in hemihydrate phosphoric acid process
Disclosed is a process for treating a waste stream containing calcium sulfate by depositing said waste stream on a gypstack, collecting the leachate from the gypstack, and recovering the P2 O5 values therefrom. Also disclosed is appa...
01/28/1992
5079390Lock-out device for circuit breakers
Disclosed is a device that can be placed on the lever arm of a switch and locked to prevent the switch from being turned on. The device comprises a rigid body having a clasping device for removably fixing the rigid body to the lever arm, an aperture throu...
01/07/1992
5077370Novel polyimidesiloxanes and methods for their preparation and use
Substantially fully imidized polyimidesiloxanes which are based on a selected pyridine compound are soluble in diglyme which gives them particular utility in the micro-electronics industry. The polymers are prepared from the dianhydride, a difunctional si...
12/31/1991
5066693Molding compositions of resole phenolic resin and epoxy resin
Phenolic molding compositions, particularly useful as sheet molding compositions comprise: 1) a resole phenole resin, 2) a thickening agent selected from the group consisting of alkaline earth metal oxides or hydroxides and silanes, 3) a filler selected f...
11/19/1991
5053106Low friction, wear resistant plastic parts
Plastic molded articles having low friction and excellent wear resistance are produced by treating the surface of the plastic article with an aqueous solution of an inorganic fluoride such as hydrogen fluoride. Plastic articles which can be made in accord...
10/01/1991
5034370Color developer for pressure-sensitive recording paper
A color developer for pressure-sensitive recording paper is produced by admising components comprising: (A) 100 parts by weight of a polyvalent metal salt of a co-condensation product of a substituted salicylic acid, an aromatic hydrocarbon and an aldehyd...
07/23/1991
5034211Reducing turbidity in chromic acid solutions
Disclosed is a method of reducing the turbidity of an aqueous solution of chromic acid which is formed by dissolving melted chromic anhydride in water. The chromic anhydride is contacted with water in an amount in excess of 0.02 wt %, but insufficient to ...
07/23/1991
5032279Separation of fluids using polyimidesiloxane membrane
Disclosed is a method of separating a first fluid from a mixture with a second fluid by placing the mixture in contact with a polyimidesiloxane membrane. The first fluid preferentially passes through the membrane, thereby separating the fluids. The polyim...
07/16/1991
5008361Crystalline polyimidesiloxanes
Novel crystalline polyimidesiloxanes are prepared by reacting BTDA, and a siloxane monomer with a diamine selected from bis-4(4-aminophenoxy) phenyl sulfone and 2,2-bis-4(4-aminophenoxy) phenyl propane. The products have low water absorption....
04/16/1991
5001250Purification of bidentate organophosphorous extractants
Crude N,N-dialkylcarbamoylmethylphosphonates and phosphine oxide extractants, and particularly crude dihexyl N,N-diethylcarbamoylmethylphosphonate and octylphenyl N,N-diisobutylcarbamoyl phosphine oxide, are purified by distilling the crude materials...
03/19/1991
4997638Production of hexametaphosphates from other phosphates
Disclosed is a method of making hexametaphosphates by reacting sodium tripolyphosphate, tetrasodium pyrophosphate, or trisodium phosphate with phosphoric acid, forming a molten glass of said mixture, and chilling said molten glass to form a solid....
03/05/1991
4997637Digestive crystallizing process and apparatus for purification of KC1
Disclosed is a method of reducing the sodium chloride content of potassium chloride by forming an aqueous slurry of potassium chloride feed crystals having a wide particle size distribution with an average diameter of about 0.1 to about 50 microns in a li...
03/05/1991
4997908Solvent resistant polymidesiloxane
Disclosed is a substantially fully imidized diglyme-insoluble, N-methylpyrrolidone-soluble polyimidesiloxane which is the reaction product of a dianhydride, about 1 to about 5% by weight of a mono-anhydride, and a mixture of about 20 to about 50% by weigh...
03/05/1991
4996278Novel polyimidesiloxanes and methods for their preparation and use based on diamines with pendant fluorine groups
Substantially fully imidized polyimidesiloxanes which are based on a selected pyridine compound are soluble in diglyme which gives them particular utility in the micro-electronics industry. The polymers are prepared from the dianhydride, a difunctional si...
02/26/1991
4994248P2 O5 recovery and phosphoric acid purification
Disclosed is an improved process for purifying phosphoric acid where a calcium sulfate hemihydrate slurry is first filtered to produce a first filtrate and a filter cake which comprises calcium sulfate hemihydrate, the calcium sulfate hemihydrate filter c...
02/19/1991
4990674Synthesis of aliphatic aromatic phosphine oxides
Disclosed is a method of making an aliphatic aromatic phosphine oxide by reacting an aliphatic aromatic phosphinic acid with a halogenating agent to produce a phosphoryl halide, reducing the phosphoryl halide to a phosphinous halide, hydrolyzing the phosp...
02/05/1991
4990670Method of making 1,1'-oxybis (3-nitro-5-trifluoromethyl)-benzene
Disclosed is a method of making 1,1'-oxybis (3-nitro-5-trifluoromethyl)-benzene by heating a nitro benzofluoride compound having the formula ##STR1## where "X" is selected from the group consisting of NO2, Cl, and F, with an alkali me...
02/05/1991
4981999Selective removal of chlorine from chlorophthalic compounds
Disclosed is a method of selectively removing chlorine atoms in the order of fifth position first, fourth position second, and third position third from a chlorophthalic compound having at least two ring chlorine atoms such as a chlorophthalic acid or a c...
01/01/1991
4978798Method of making halobenzophenones and intermediates thereof
Disclosed is a method of making a bisphenyl dihalomethane by reacting a trihalomethylbenzene with a halobenzene and a Lewis acid. The bisphenyl dihalomethane can than be reacted with water to form a halobenzophenone. In an optical third step ring chlorine...
12/18/1990
4975323Ferrophosphorus particles treated with hypophosphorous acid
The conductivity of ground ferrophosphorus particles is increased by contacting the particles with an aqueous solution of hypophosphorus acid, preferably at a temperature between room temperature and about 50°C. The particles are then washed and dried an...
12/04/1990
4967838Oil well and method using completion fluid
Disclosed is a method of preventing fluids in the ground from rising around an oil well pipe by filling the space around the pipe with an oil well completion fluid comprising water, about 50 to about 65% by weight, based on total fluid weight, of dipotass...
11/06/1990
4954639Single pot process for making a fluoroanthranilic acid
Disclosed is a method of making ionized fluoroanthranilic acid from a fluorophthalic compound in a single pot process without isolating any intermediate product. A composition is prepared which comprises an aqueous solution of water, a fluorophthalic comp...
09/04/1990
4935213Zero discharge process for preparing potassium tripolyphosphate
Disclosed is a method of making potassium tripolyphosphate by loading an ion exchange resin with either potassium or hydrogen ions and passing an aqueous solution of sodium tripolyphosphate through the resin so that the sodium ions of the sodium tripolyph...
06/19/1990
4922012Compositions of matter comprising dialkyl-(N,N-dialkylcarbamoylmethyl) phosphine oxides
Novel organic tertiary phosphine oxides for example, bidentate organophosphorus actinide extractants, such as the carbamoylmethylphosphine oxides (CMPO's) are disclosed, such compounds can be prepared (e.g., in 85% or better yield and purity) by a process...
05/01/1990
4906522Compounds of nickel, iron and phosphorus
Compositions of nickel, iron and phosphorus, are prepared by fusing nickel and ferrophosphorus in an inert atmosphere, with the nickel preferably comprising from about 5% to about 70% by weight of the composition. The fused composition is ground or atomiz...
03/06/1990
 
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